Analytical Chemistry Laboratory (ACL) procedure compendium. Volume 2, Sample preparation methods

Technical Report · Sun Aug 01 04:00:00 EDT 1993

DOI:https://doi.org/10.2172/10178321· OSTI ID:10178321

This volume contains the interim change notice for sample preparation methods. Covered are: acid digestion for metals analysis, fusion of Hanford tank waste solids, water leach of sludges/soils/other solids, extraction procedure toxicity (simulate leach in landfill), sample preparation for gamma spectroscopy, acid digestion for radiochemical analysis, leach preparation of solids for free cyanide analysis, aqueous leach of solids for anion analysis, microwave digestion of glasses and slurries for ICP/MS, toxicity characteristic leaching extraction for inorganics, leach/dissolution of activated metal for radiochemical analysis, extraction of single-shell tank (SST) samples for semi-VOC analysis, preparation and cleanup of hydrocarbon- containing samples for VOC and semi-VOC analysis, receiving of waste tank samples in onsite transfer cask, receipt and inspection of SST samples, receipt and extrusion of core samples at 325A shielded facility, cleaning and shipping of waste tank samplers, homogenization of solutions/slurries/sludges, and test sample preparation for bioassay quality control program.

• Research Organization: Pacific Northwest Lab., Richland, WA (United States)
• Sponsoring Organization: USDOE, Washington, DC (United States)
• DOE Contract Number: AC06-76RL01830
• OSTI ID: 10178321
• Report Number(s): PNL-MA--599-Vol.2; ON: DE93019190
• Country of Publication: United States
• Language: English

Related Subjects

052002
12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE WASTES FROM NUCLEAR FACILITIES
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400101
ACTIVATION, NUCLEAR REACTION, RADIOMETRIC, AND RADIOCHEMICAL PROCEDURES
BATTELLE PACIFIC NORTHWEST LABORATORIES
CASKS
CHEMICAL ANALYSIS
DIGESTION
DISSOLUTION
LEACHING
ORGANIC COMPOUNDS
RADIOACTIVE WASTE STORAGE
RADIOACTIVE WASTES
RADIOCHEMICAL ANALYSIS
SAMPLE PREPARATION
SLUDGES
SLURRIES
SOLIDS
SOLUTIONS
TANKS
VOLATILE MATTER
WASTE DISPOSAL AND STORAGE