skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Analytical and experimental evaluation of joining silicon nitride to metal and silicon carbide to metal for advanced heat engine applications. Final report

Technical Report ·
DOI:https://doi.org/10.2172/10176461· OSTI ID:10176461
; ; ;  [1];  [2]
  1. GTE Labs., Inc., Waltham, MA (US)
  2. Brown Univ., Providence, RI (US). Div. of Engineering

This report summarizes the results of Phase 2 of Analytical and Experimental Evaluation of Joining Silicon Nitride to Metal and Silicon Carbide to Metal for Advanced Heat Engine Applications. A general methodology was developed to optimize the joint geometry and material systems for 650{degrees}C applications. Failure criteria were derived to predict the fracture of the braze and ceramic. Extensive finite element analyses (FEA) were performed to examine various joint geometries and to evaluate the affect of different interlayers on the residual stress state. Also, material systems composed of coating materials, interlayers, and braze alloys were developed for the program based on the chemical stability and strength of the joints during processing, and service. The FEA results were compared with experiments using two methods: (1) an idealized strength relationship of the ceramic, and (2) a probabilistic analysis of the ceramic strength (NASA CARES). The results showed that the measured strength of the joint reached 30--80% of the strength predicted by FEA. Also, potential high-temperature braze alloys were developed and evaluated for the high-temperature application of ceramic-metal joints. 38 tabs, 29 figs, 20 refs.

Research Organization:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); GTE Labs., Inc., Waltham, MA (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC05-84OR21400
OSTI ID:
10176461
Report Number(s):
ORNL/Sub-90-SB047/2; ON: DE93018128; TRN: 93:002864
Resource Relation:
Other Information: PBD: May 1993
Country of Publication:
United States
Language:
English