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A design of experiment study of plasma sprayed alumina-titania coatings

Conference ·
OSTI ID:10165288
 [1]; ;  [2];  [3]; ;  [4]
  1. Du Pont de Nemours (E.I.) and Co., Aiken, SC (United States). Savannah River Lab.
  2. EG and G Idaho, Inc., Idaho Falls, ID (United States)
  3. Tubal Cain Co., Loveland, OH (United States)
  4. Metco/Perkin-Elmer, Westbury, NY (United States)

An experimental study of the plasma spraying of alumina-titania powder is presented in this paper. This powder system is being used to fabricate heater tubes that emulate nuclear fuel tubes for use in thermal-hydraulic testing. Coating experiments were conducted using a Taguchi fractional-factorial design parametric study. Operating parameters were varied around the typical spray parameters in a systematic design of experiments in order to display the range of plasma processing conditions and their effect on the resultant coating. The coatings were characterized by hardness and electrical tests, image analysis, and optical metallography. Coating qualities are discussed with respect to dielectric strength, hardness, porosity, surface roughness, deposition efficiency, and microstructure. The attributes of the coatings are correlated with the changes in operating parameters.

Research Organization:
EG and G Idaho, Inc., Idaho Falls, ID (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC07-76ID01570
OSTI ID:
10165288
Report Number(s):
EGG-M--92006; CONF-9206135--5; ON: DE92017877
Country of Publication:
United States
Language:
English