Tank 241-SX-105 rotary mode core sampling and analysis plan
This sampling and analysis plan (SAP) identifies characterization objectives pertaining to sample collection, laboratory analytical evaluation, and reporting requirements for rotary mode core samples from tank 241-SX-105 (SX-105). It is written in accordance with Tank Safety Screening Data Quality Objective (Dukelow et al. 1995) and Memorandum of Understanding for the Organic Complexant Safety Issue Data Requirements (Schreiber 1997a). Vapor screening issues apply as well, but are outside the scope of this SAP. A physical profile prediction based on waste fill history and previous sampling information is provided in Appendix A. Prior to core sampling, the dome space (below the riser) shall be measured for the presence of flammable gases. The measurement shall be taken from within the dome space and the data reported as a percentage of the lower flammability limit (LFL). The results shall be transmitted to the tank coordinator within ten working days of the sampling event (Schreiber 1997b). If the results are above 25 percent of the LFL when analyzing by gas chromatography/mass spectrometry or gas-specific monitoring gauges or above 10% of the LFL when analyzing with a combustible gas meter, the necessity for recurring sampling for flammable gas concentration and the frequency of such sampling will be determined by the Flammable Gas Safety Project. Any additional vapor sampling is not within the scope of this SAP.
- Research Organization:
- Fluor Daniel Hanford Inc., Richland, WA (United States)
- Sponsoring Organization:
- USDOE Office of Environmental Restoration and Waste Management, Washington, DC (United States)
- DOE Contract Number:
- AC06-96RL13200
- OSTI ID:
- 10154145
- Report Number(s):
- HNF--2107; ON: DE99050468; BR: EW3130000
- Country of Publication:
- United States
- Language:
- English
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054000
11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS
12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE WASTES FROM NUCLEAR FACILITIES
CHEMICAL ANALYSIS
GAS ANALYSIS
HANFORD RESERVATION
HEALTH AND SAFETY
ORGANIC COMPOUNDS
PLANNING
RADIOACTIVE WASTES
SAFETY ENGINEERING
SAMPLING
STORAGE FACILITIES
WASTE DISPOSAL AND STORAGE