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U.S. Department of Energy
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Polychlorinated biphenyls (PCB) analysis report for solid sample from 219S tank 104

Technical Report ·
DOI:https://doi.org/10.2172/10148859· OSTI ID:10148859

A sample of solids was obtained from tank 104 of 219S via a peristaltic pump equipped with a stainless steel tube and Norprenel tubing (Phthalate free). The sample obtained in a glass jar with Teflon 2 lid, was analyzed for PCBs as Aroclor mixtures. A soxhlet extraction procedure was used to extract the Aroclors from the sample. Analysis was performed using dual column confirmation gas chromatography/electron capture detection (GC/ECD). The extraction method closely follows SW-846 method 3540C and the analysis follows SW-846 method.

Research Organization:
Fluor Daniel Hanford Inc., Richland, WA (United States)
Sponsoring Organization:
USDOE Office of Environmental Restoration and Waste Management, Washington, DC (United States)
DOE Contract Number:
AC06-96RL13200
OSTI ID:
10148859
Report Number(s):
HNF-SD-WM-DP--297; ON: DE99050612; BR: EW3120074
Country of Publication:
United States
Language:
English