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Title: Polychlorinated biphenyls (PCB) analysis report for solid sample from 219S tank 104

Abstract

A sample of solids was obtained from tank 104 of 219S via a peristaltic pump equipped with a stainless steel tube and Norprenel tubing (Phthalate free). The sample obtained in a glass jar with Teflon 2 lid, was analyzed for PCBs as Aroclor mixtures. A soxhlet extraction procedure was used to extract the Aroclors from the sample. Analysis was performed using dual column confirmation gas chromatography/electron capture detection (GC/ECD). The extraction method closely follows SW-846 method 3540C and the analysis follows SW-846 method.

Authors:
Publication Date:
Research Org.:
Fluor Daniel Hanford Inc., Richland, WA (United States)
Sponsoring Org.:
USDOE Office of Environmental Restoration and Waste Management, Washington, DC (United States)
OSTI Identifier:
10148859
Report Number(s):
HNF-SD-WM-DP-297
ON: DE99050612; BR: EW3120074; TRN: AHC29927%%235
DOE Contract Number:
AC06-96RL13200
Resource Type:
Technical Report
Resource Relation:
Other Information: PBD: 27 Mar 1998
Country of Publication:
United States
Language:
English
Subject:
12 MANAGEMENT OF RADIOACTIVE AND NON-RADIOACTIVE WASTES FROM NUCLEAR FACILITIES; HANFORD RESERVATION; RADIOACTIVE WASTE STORAGE; STORAGE FACILITIES; SAMPLING; POLYCHLORINATED BIPHENYLS; GAS CHROMATOGRAPHY; ELECTRON CAPTURE; 052002; WASTE DISPOSAL AND STORAGE

Citation Formats

Ross, G.A.. Polychlorinated biphenyls (PCB) analysis report for solid sample from 219S tank 104. United States: N. p., 1998. Web. doi:10.2172/10148859.
Ross, G.A.. Polychlorinated biphenyls (PCB) analysis report for solid sample from 219S tank 104. United States. doi:10.2172/10148859.
Ross, G.A.. Fri . "Polychlorinated biphenyls (PCB) analysis report for solid sample from 219S tank 104". United States. doi:10.2172/10148859. https://www.osti.gov/servlets/purl/10148859.
@article{osti_10148859,
title = {Polychlorinated biphenyls (PCB) analysis report for solid sample from 219S tank 104},
author = {Ross, G.A.},
abstractNote = {A sample of solids was obtained from tank 104 of 219S via a peristaltic pump equipped with a stainless steel tube and Norprenel tubing (Phthalate free). The sample obtained in a glass jar with Teflon 2 lid, was analyzed for PCBs as Aroclor mixtures. A soxhlet extraction procedure was used to extract the Aroclors from the sample. Analysis was performed using dual column confirmation gas chromatography/electron capture detection (GC/ECD). The extraction method closely follows SW-846 method 3540C and the analysis follows SW-846 method.},
doi = {10.2172/10148859},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Fri Mar 27 00:00:00 EST 1998},
month = {Fri Mar 27 00:00:00 EST 1998}
}

Technical Report:

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