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Tortuous path chemical preconcentrator

Patent ·
OSTI ID:1014661

A non-planar, tortuous path chemical preconcentrator has a high internal surface area having a heatable sorptive coating that can be used to selectively collect and concentrate one or more chemical species of interest from a fluid stream that can be rapidly released as a concentrated plug into an analytical or microanalytical chain for separation and detection. The non-planar chemical preconcentrator comprises a sorptive support structure having a tortuous flow path. The tortuosity provides repeated twists, turns, and bends to the flow, thereby increasing the interfacial contact between sample fluid stream and the sorptive material. The tortuous path also provides more opportunities for desorption and readsorption of volatile species. Further, the thermal efficiency of the tortuous path chemical preconcentrator is comparable or superior to the prior non-planar chemical preconcentrator. Finally, the tortuosity can be varied in different directions to optimize flow rates during the adsorption and desorption phases of operation of the preconcentrator.

Research Organization:
Sandia Corporation (Albuquerque, NM)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC04-94AL85000
Assignee:
Sandia Corporation (Albuquerque, NM)
Patent Number(s):
7,799,280
Application Number:
US Patent Application 11/355,480
OSTI ID:
1014661
Country of Publication:
United States
Language:
English

References (3)

Recent advancements in the gas-phase MicroChemLab conference December 2004
Nanoporous-carbon films for microsensor preconcentrators journal May 2002
Template-Based Approaches to the Preparation of Amorphous, Nanoporous Silicas August 1996

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