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U.S. Department of Energy
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Reaction of formic and nitric acids with Savannah River Site radioactive HLW sludge in the DWPF pretreatment steps

Conference ·
OSTI ID:10128077
; ;  [1];  [2]
  1. Westinghouse Savannah River Co., Aiken, SC (United States)
  2. Vanderbilt Univ., Nashville, TN (United States)

The Defense Waste Processing Facility (DWPF) at the Savannah River Site (SRS) will combine borosilicate frit with highly radioactive waste sludge to produce glass waste forms for disposal. A key step in the DWPF will be acidification of the sludge with formic and nitric acids prior to vitrification. The reducing properties of formic acid will be used to reduce mercury (II) oxide and salts to elemental mercury. The mercury will then be steam-stripped, recovered, and purified. Another benefit of acidifying the sludge will be to reduce its viscosity so that a sludge-frit mixture can be pumped to the melter. The sludge viscosity decreases with pH as various sludge components dissolve with increasing acidity.

Research Organization:
Westinghouse Savannah River Co., Aiken, SC (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC09-89SR18035
OSTI ID:
10128077
Report Number(s):
WSRC-MS--93-563; CONF-940225--42; ON: DE94007279
Country of Publication:
United States
Language:
English