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Title: Feasibility of ceramic joining with high energy electron beams

Conference ·
OSTI ID:10106995
; ; ; ;  [1];  [2]
  1. Sandia National Labs., Albuquerque, NM (United States)
  2. Titan Corp., Albuquerque, NM (United States)

Joining structural ceramics is possible using high melting point metals such as Mo and Pt that are heated with a high energy electron beam, with the potential for producing joints with high temperature capability. A 10 MeV electron beam can penetrate through 1 cm of ceramic, offering the possibility of buried interface joining. Because of transient heating and the lower heat capacity of the metal relative to the ceramic, a pulsed high power beam has the potential for melting the metal without decomposing or melting the adjacent ceramic. The authors have demonstrated the feasibility of the process with a series of 10 MeV, 1 kW electron beam experiments. Shear strengths up to 28 NTa have been measured for Si{sub 3}N{sub 4}-Mo-Si{sub 3}N{sub 4}. These modest strengths are due to beam non-uniformity and the limited area of bonding. The bonding mechanism appears to be a thin silicide reaction layer. Si{sub 3}N{sub 4}-Si{sub 3}N{sub 4} joints with no metal layer were also produced, apparently bonded an yttrium apatite grain boundary phase.

Research Organization:
Sandia National Labs., Albuquerque, NM (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC04-94AL85000
OSTI ID:
10106995
Report Number(s):
SAND-94-2056C; CONF-950129-1; ON: DE95004519; TRN: 95:000820
Resource Relation:
Conference: 19. annual conference on advanced ceramics, materials and structures,Cocoa Beach, FL (United States),9-12 Jan 1995; Other Information: PBD: [1995]
Country of Publication:
United States
Language:
English

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