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Title: Facilities for high-pressure research with the diamond anvil cell at GSECARS

Abstract

An overview of facilities for high-pressure research with the diamond anvil cell (DAC) at the GeoSoilEnviroCARS (GSECARS) sector at the Advanced Photon Source (Argonne, Illinois) is presented. There are three operational experimental stations (13-ID-C, 13-ID-D and 13-BM-D) where DAC instrumentation is installed for various types of experiments at high pressure and extreme temperature conditions. A fourth station (13-BM-C) is under construction and will be operational in 2006. While most X-ray diffraction experiments have been undertaken with powder samples so far, there is a growing demand for single-crystal diffraction (SCD) at high pressure. As one of the principal components at GSECARS, SCD is currently under rapid development. Other relevant techniques have also been developed for obtaining complementary information from powder or single-crystal samples at high pressure. For example, an on-line Brillouin system is installed and operational at 13-BM-D for acoustic velocity and single-crystal elasticity determinations. In addition, various X-ray spectroscopy techniques (e.g. X-ray emission and X-ray Raman) are employed for measuring electronic and magnetic properties. Future developments are discussed with the DAC program at GSECARS.

Authors:
; ; ; ;  [1]
  1. UC
Publication Date:
Research Org.:
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Sponsoring Org.:
USDOE
OSTI Identifier:
1008548
Resource Type:
Journal Article
Journal Name:
J. Synchrotron Rad.
Additional Journal Information:
Journal Volume: 12; Journal Issue: (5) ; 2005; Journal ID: ISSN 0909-0495
Country of Publication:
United States
Language:
ENGLISH
Subject:
43 PARTICLE ACCELERATORS; ACOUSTICS; ADVANCED PHOTON SOURCE; CONSTRUCTION; DIAMONDS; DIFFRACTION; ELASTICITY; MAGNETIC PROPERTIES; VELOCITY; X-RAY DIFFRACTION; X-RAY SPECTROSCOPY

Citation Formats

Shen, G, Prakapenka, V B, Eng, P J, Rivers, M L, and Sutton, S R. Facilities for high-pressure research with the diamond anvil cell at GSECARS. United States: N. p., 2010. Web.
Shen, G, Prakapenka, V B, Eng, P J, Rivers, M L, & Sutton, S R. Facilities for high-pressure research with the diamond anvil cell at GSECARS. United States.
Shen, G, Prakapenka, V B, Eng, P J, Rivers, M L, and Sutton, S R. Tue . "Facilities for high-pressure research with the diamond anvil cell at GSECARS". United States.
@article{osti_1008548,
title = {Facilities for high-pressure research with the diamond anvil cell at GSECARS},
author = {Shen, G and Prakapenka, V B and Eng, P J and Rivers, M L and Sutton, S R},
abstractNote = {An overview of facilities for high-pressure research with the diamond anvil cell (DAC) at the GeoSoilEnviroCARS (GSECARS) sector at the Advanced Photon Source (Argonne, Illinois) is presented. There are three operational experimental stations (13-ID-C, 13-ID-D and 13-BM-D) where DAC instrumentation is installed for various types of experiments at high pressure and extreme temperature conditions. A fourth station (13-BM-C) is under construction and will be operational in 2006. While most X-ray diffraction experiments have been undertaken with powder samples so far, there is a growing demand for single-crystal diffraction (SCD) at high pressure. As one of the principal components at GSECARS, SCD is currently under rapid development. Other relevant techniques have also been developed for obtaining complementary information from powder or single-crystal samples at high pressure. For example, an on-line Brillouin system is installed and operational at 13-BM-D for acoustic velocity and single-crystal elasticity determinations. In addition, various X-ray spectroscopy techniques (e.g. X-ray emission and X-ray Raman) are employed for measuring electronic and magnetic properties. Future developments are discussed with the DAC program at GSECARS.},
doi = {},
journal = {J. Synchrotron Rad.},
issn = {0909-0495},
number = (5) ; 2005,
volume = 12,
place = {United States},
year = {2010},
month = {7}
}