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Pressure-induced phase transformations in cubic Gd[subscript 2]O[subscript 3]

Journal Article · · J. Appl. Phys.
DOI:https://doi.org/10.1063/1.3236580· OSTI ID:1005918

High-pressure transformation and compression behavior of Gd{sub 2}O{sub 3} were investigated using synchrotron radiation x-ray diffraction in a diamond anvil cell up to 44 GPa at room temperature. The structural transformation from a cubic to a monoclinic phase occurred during the sample precompression process. Phase transitions from both the cubic and the monoclinic polymorphs to a hexagonal structure were observed. The hexagonal phase was stable up to the highest pressure in this study and was not quenchable and transformed to a monoclinic phase after pressure release. The bulk moduli of Gd{sub 2}O{sub 3} for the cubic, monoclinic, and hexagonal phases were obtained by fitting the compression data to the Birch-Murnaghan equation of state. Moreover, an anomaly of the hexagonal type Gd{sub 2}O{sub 3} was observed.

Research Organization:
Argonne National Laboratory (ANL)
Sponsoring Organization:
USDOE
OSTI ID:
1005918
Journal Information:
J. Appl. Phys., Journal Name: J. Appl. Phys. Journal Issue: (7) ; 10, 2009 Vol. 106; ISSN JAPIAU; ISSN 0021-8979
Country of Publication:
United States
Language:
ENGLISH

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