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Title: Existing technology transfer report: analytical capabilities. Appendix B. Volume 3

Technical Report ·
DOI:https://doi.org/10.2172/6615333· OSTI ID:6615333

The overall objective of the on-going analytical efforts was to develop in-house expertise and analytical capability for the analysis of coal and coal-derived products in support of SRC-I process technology. The approach taken and work accomplished involved: identification of test methods and associated equipment; review and implementation of analytical facility plan; evaluation of existing instrumentation; evaluation and purchase of new instruments; training of laboratory personnel; validation or development of analytical methods; development of standard product work-up methods and development of analytical protocol for detailed characterization of SRC-I solid and liquid products. This volume contains Appendix B with the following attachments: solvent separation procedure A; Wilsonville solvent separation procedure, distillation separation procedure; solvent separation modified Wilsonville Procedure W; statistical comparison of 3 solvent separation procedures; methods development for column chromatography, and application of gas chromatography to characterization of a hydrogen donor solvent; and high performance liquid chromatographic procedure.

Research Organization:
Air Products and Chemicals, Inc., Allentown, PA (USA)
DOE Contract Number:
AC05-78OR03054
OSTI ID:
6615333
Report Number(s):
DOE/OR/03054-116-Vol.3; ON: DE85001636
Resource Relation:
Other Information: Portions are illegible in microfiche products. Original copy available until stock is exhausted
Country of Publication:
United States
Language:
English