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Title: Titanium carbide (TiC) nano-fibrous felts

Patent ·
OSTI ID:1600443

A method of synthesizing mechanically resilient titanium carbide (TiC) nanofibrous felts comprising continuous nanofibers or nano-ribbons with TiC crystallites embedded in carbon matrix, comprising: (a) electrospinning a spin dope for making precursor nanofibers with diameters less than 0.5 J.Lm; (b) overlaying the nanofibers to produce a nano-fibrous mat (felt); and then (c) heating the nano-felts first at a low temperature, and then at a high temperature for making electrospun continuous nanofibers or nano-ribbons with TiC crystallites embedded in carbon matrix; and (d) chlorinating the above electrospun nano-felts at an elevated temperature to remove titanium for producing carbide derived carbon (CDC) nano-fibrous felt with high specific surface areas.

Research Organization:
South Dakota Board of Regents, Pierre, SD (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
FG02-08ER64624
Assignee:
South Dakota Board of Regents (Pierre, SD)
Patent Number(s):
10,519,580
Application Number:
14/551,348
OSTI ID:
1600443
Resource Relation:
Patent File Date: 11/24/2014
Country of Publication:
United States
Language:
English

References (9)

Synthesis of continuous TiC nanofibers and/or nanoribbons through electrospinning followed by carbothermal reduction journal January 2010
Chemically Modified Organic CDC Based Rapid Analysis System patent-application May 2010
Nanoelectronic Devices Based on Nanowire Networks patent-application December 2006
Graphite Electrode for Electrothermic Reduction Furnaces, Electrode Column, and Method of Producing Graphite Electrodes patent-application November 2005
Process for Producing Nanoporous Carbide-Derived Carbons with Increased Gas Storage Capability patent-application December 2009
NANOFIBER AND PREPARATION METHOD THEREOF patent-application June 2011
Process for Manufacturing Carbon Coated Nanoparticles of a Transition Metal Oxide patent-application August 2010
Titanium carbide derived nanoporous carbon for energy-related applications journal October 2006
Preparation of interstitial titanium ceramic fibers patent June 1990