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Title: Flexible sample environment for high resolution neutron imaging at high temperatures in controlled atmosphere

Journal Article · · Review of Scientific Instruments
DOI:https://doi.org/10.1063/1.4937615· OSTI ID:1261503

In high material penetration by neutrons allows for experiments using sophisticated sample environments providing complex conditions. Thus, neutron imaging holds potential for performing in situ nondestructive measurements on large samples or even full technological systems, which are not possible with any other technique. Our paper presents a new sample environment for in situ high resolution neutron imaging experiments at temperatures from room temperature up to 1100 degrees C and/or using controllable flow of reactive atmospheres. The design also offers the possibility to directly combine imaging with diffraction measurements. Design, special features, and specification of the furnace are described. In addition, examples of experiments successfully performed at various neutron facilities with the furnace, as well as examples of possible applications are presented. Our work covers a broad field of research from fundamental to technological investigations of various types of materials and components.

Research Organization:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States). Spallation Neutron Source (SNS)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
1261503
Journal Information:
Review of Scientific Instruments, Vol. 86, Issue 12; ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)Copyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 10 works
Citation information provided by
Web of Science

References (31)

Highly absorbing gadolinium test device to characterize the performance of neutron imaging detector systems journal May 2007
Optimization of Timepix count rate capabilities for the applications with a periodic input signal journal May 2014
Phase Transition Mapping by Means of Neutron Imaging in SOFC Anode Supports during Reduction under Applied Stress journal June 2015
A review of advanced techniques for characterising SOFC behaviour journal December 2009
Kinetics of Hydrogen Absorption and Release in Zirconium Alloys During Steam Oxidation journal July 2008
Characterization of textured materials by TOF transmission journal November 2006
Neutron Scattering at Highest Magnetic Fields at the Helmholtz Centre Berlin journal January 2010
Engineering applications of Bragg-edge neutron transmission journal December 2002
Neutron radiography with sub-15μm resolution through event centroiding
  • Tremsin, Anton S.; McPhate, Jason B.; Vallerga, John V.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 688 https://doi.org/10.1016/j.nima.2012.06.005
journal October 2012
High-Resolution Strain Mapping Through Time-of-Flight Neutron Transmission Diffraction with a Microchannel Plate Neutron Counting Detector: High-Resolution Strain Mapping journal September 2011
Time-of-flight neutron imaging at a continuous source: Proof of principle using a scintillator CCD imaging detector
  • Strobl, M.; Hilger, A.; Boin, M.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 651, Issue 1 https://doi.org/10.1016/j.nima.2010.12.121
journal September 2011
In-situ observations of catalytic surface reactions with soft x-rays under working conditions journal February 2015
In-situ investigation of hydrogen diffusion in Zircaloy-4 by means of neutron radiography journal February 2012
Neutron imaging in materials science journal June 2011
Electrode materials and reaction mechanisms in solid oxide fuel cells: a brief review. III. Recent trends and selected methodological aspects journal April 2011
Solid oxide fuel cells (SOFCs): a review of an environmentally clean and efficient source of energy journal October 2002
Heterogeneous Catalyst Deactivation and Regeneration: A Review journal February 2015
Effect of stress on NiO reduction in solid oxide fuel cells: a new application of energy-resolved neutron imaging journal March 2015
3D Mapping of Crystallographic Phase Distribution using Energy-Selective Neutron Tomography journal April 2014
Quantitative determination of absorbed hydrogen in oxidised zircaloy by means of neutron radiography
  • Grosse, M.; Lehmann, E.; Vontobel, P.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 566, Issue 2 https://doi.org/10.1016/j.nima.2006.06.038
journal October 2006
Time-of-flight neutron imaging for spatially resolved strain investigations based on Bragg edge transmission at a reactor source
  • Strobl, M.; Woracek, R.; Kardjilov, N.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 680 https://doi.org/10.1016/j.nima.2012.04.026
journal July 2012
Advances in neutron radiography and tomography journal November 2009
Manufacturing of Anode-Supported SOFC's: Processing Parameters and their Influence
  • Ramousse, Severine; Menon, Mohan; Brodersen, Karen
  • 10th International Symposium on Solid Oxide Fuel Cells (SOFC-X), ECS Transactions https://doi.org/10.1149/1.2729107
conference January 2007
Transmission Bragg edge spectroscopy measurements at ORNL Spallation Neutron Source journal November 2010
Influence of oxide layer morphology on hydrogen concentration in tin and niobium containing zirconium alloys after high temperature steam oxidation journal March 2009
High-temperature furnace for dynamic neutron radiography journal August 2003
New trends in neutron imaging
  • Kardjilov, Nikolay; Hilger, André; Manke, Ingo
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 605, Issue 1-2 https://doi.org/10.1016/j.nima.2009.01.162
journal June 2009
Energy-selective neutron transmission imaging at a pulsed source
  • Kockelmann, W.; Frei, G.; Lehmann, E. H.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 578, Issue 2 https://doi.org/10.1016/j.nima.2007.05.207
journal August 2007
In-situ neutron radiography investigations of hydrogen diffusion and absorption in zirconium alloys
  • Grosse, M.; van den Berg, M.; Goulet, C.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 651, Issue 1 https://doi.org/10.1016/j.nima.2010.12.070
journal September 2011
Neutron imaging options at the BOA beamline at Paul Scherrer Institut
  • Morgano, M.; Peetermans, S.; Lehmann, E. H.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 754 https://doi.org/10.1016/j.nima.2014.03.055
journal August 2014
Detection system for microimaging with neutrons journal February 2012

Cited By (1)

In situ time-of-flight neutron imaging of NiO–YSZ anode support reduction under influence of stress journal September 2016