Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells
Abstract
Here, we report measurements of the temperature- and pressure-dependent resistance, R(T, p), of a manganin manometer in a 4He-gas pressure setup from room temperature down to the solidification temperature of 4He (Tsolid ~ 50 K at 0.8 GPa) for pressures, p, between 0 GPa and ~0.8 GPa. The same manganin wire manometer was also measured in a piston-cylinder cell (PCC) from 300 K down to 1.8 K and for pressures between 0 GPa and ~2 GPa. From these data, we infer the temperature and pressure dependence of the pressure coefficient of manganin, α(T, p), defined by the equation Rp = (1 + αp)R0, where R0 and Rp are the resistances of manganin at ambient pressure and finite pressure, respectively. Our results indicate that upon cooling, α first decreases, then goes through a broad minimum at ~120 K, and increases again toward lower temperatures. In addition, we find that α is almost pressure-independent at T ≳ 60 K up to p ~ 2 GPa, but shows a pronounced p dependence at T ≲ 60 K. Using this manganin manometer, we demonstrate that p overall decreases with decreasing temperature in the PCC for the full pressure range and that the size ofmore »
- Authors:
-
- Ames Lab., Ames, IA (United States); Iowa State Univ., Ames, IA (United States)
- Iowa State Univ., Ames, IA (United States); Universidade Federal do ABC (UFABC), Santo André, SP (Brazil)
- Goethe Univ., Frankfurt (Germany)
- Publication Date:
- Research Org.:
- Ames Laboratory (AMES), Ames, IA (United States); Iowa State Univ., Ames, IA (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division; Gordon and Betty Moore Foundation
- OSTI Identifier:
- 1670358
- Alternate Identifier(s):
- OSTI ID: 1657639
- Report Number(s):
- IS-J-10,326
Journal ID: ISSN 0034-6748; TRN: US2204193
- Grant/Contract Number:
- AC02-07CH11358; GBMF4411; SFB/TR 288
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Review of Scientific Instruments
- Additional Journal Information:
- Journal Volume: 91; Journal Issue: 9; Journal ID: ISSN 0034-6748
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 47 OTHER INSTRUMENTATION; Measuring instruments; Calibration methods; Electrical properties and parameters; Sensors
Citation Formats
Xiang, Li, Gati, Elena, Bud’ko, Sergey L., Ribeiro, Raquel A., Ata, Arif, Tutsch, Ulrich, Lang, Michael, and Canfield, Paul C. Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells. United States: N. p., 2020.
Web. doi:10.1063/5.0022650.
Xiang, Li, Gati, Elena, Bud’ko, Sergey L., Ribeiro, Raquel A., Ata, Arif, Tutsch, Ulrich, Lang, Michael, & Canfield, Paul C. Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells. United States. https://doi.org/10.1063/5.0022650
Xiang, Li, Gati, Elena, Bud’ko, Sergey L., Ribeiro, Raquel A., Ata, Arif, Tutsch, Ulrich, Lang, Michael, and Canfield, Paul C. Thu .
"Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells". United States. https://doi.org/10.1063/5.0022650. https://www.osti.gov/servlets/purl/1670358.
@article{osti_1670358,
title = {Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells},
author = {Xiang, Li and Gati, Elena and Bud’ko, Sergey L. and Ribeiro, Raquel A. and Ata, Arif and Tutsch, Ulrich and Lang, Michael and Canfield, Paul C.},
abstractNote = {Here, we report measurements of the temperature- and pressure-dependent resistance, R(T, p), of a manganin manometer in a 4He-gas pressure setup from room temperature down to the solidification temperature of 4He (Tsolid ~ 50 K at 0.8 GPa) for pressures, p, between 0 GPa and ~0.8 GPa. The same manganin wire manometer was also measured in a piston-cylinder cell (PCC) from 300 K down to 1.8 K and for pressures between 0 GPa and ~2 GPa. From these data, we infer the temperature and pressure dependence of the pressure coefficient of manganin, α(T, p), defined by the equation Rp = (1 + αp)R0, where R0 and Rp are the resistances of manganin at ambient pressure and finite pressure, respectively. Our results indicate that upon cooling, α first decreases, then goes through a broad minimum at ~120 K, and increases again toward lower temperatures. In addition, we find that α is almost pressure-independent at T ≳ 60 K up to p ~ 2 GPa, but shows a pronounced p dependence at T ≲ 60 K. Using this manganin manometer, we demonstrate that p overall decreases with decreasing temperature in the PCC for the full pressure range and that the size of the pressure difference between room temperature and low temperatures (T = 1.8 K), Δp, decreases with increasing pressure. We also compare the pressure values inferred from the manganin manometer with the low-temperature pressure, determined from the superconducting transition temperature of elemental lead (Pb). As a result of these data and analysis, we propose a practical algorithm to infer the evolution of pressure with temperature in a PCC.},
doi = {10.1063/5.0022650},
journal = {Review of Scientific Instruments},
number = 9,
volume = 91,
place = {United States},
year = {Thu Sep 03 00:00:00 EDT 2020},
month = {Thu Sep 03 00:00:00 EDT 2020}
}
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