DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells

Abstract

Here, we report measurements of the temperature- and pressure-dependent resistance, R(T, p), of a manganin manometer in a 4He-gas pressure setup from room temperature down to the solidification temperature of 4He (Tsolid ~ 50 K at 0.8 GPa) for pressures, p, between 0 GPa and ~0.8 GPa. The same manganin wire manometer was also measured in a piston-cylinder cell (PCC) from 300 K down to 1.8 K and for pressures between 0 GPa and ~2 GPa. From these data, we infer the temperature and pressure dependence of the pressure coefficient of manganin, α(T, p), defined by the equation Rp = (1 + αp)R0, where R0 and Rp are the resistances of manganin at ambient pressure and finite pressure, respectively. Our results indicate that upon cooling, α first decreases, then goes through a broad minimum at ~120 K, and increases again toward lower temperatures. In addition, we find that α is almost pressure-independent at T ≳ 60 K up to p ~ 2 GPa, but shows a pronounced p dependence at T ≲ 60 K. Using this manganin manometer, we demonstrate that p overall decreases with decreasing temperature in the PCC for the full pressure range and that the size ofmore » the pressure difference between room temperature and low temperatures (T = 1.8 K), Δp, decreases with increasing pressure. We also compare the pressure values inferred from the manganin manometer with the low-temperature pressure, determined from the superconducting transition temperature of elemental lead (Pb). As a result of these data and analysis, we propose a practical algorithm to infer the evolution of pressure with temperature in a PCC.« less

Authors:
ORCiD logo [1]; ORCiD logo [1];  [1];  [2]; ORCiD logo [3];  [3];  [3];  [1]
  1. Ames Lab., Ames, IA (United States); Iowa State Univ., Ames, IA (United States)
  2. Iowa State Univ., Ames, IA (United States); Universidade Federal do ABC (UFABC), Santo André, SP (Brazil)
  3. Goethe Univ., Frankfurt (Germany)
Publication Date:
Research Org.:
Ames Laboratory (AMES), Ames, IA (United States); Iowa State Univ., Ames, IA (United States)
Sponsoring Org.:
USDOE Office of Science (SC), Basic Energy Sciences (BES). Materials Sciences & Engineering Division; Gordon and Betty Moore Foundation
OSTI Identifier:
1670358
Alternate Identifier(s):
OSTI ID: 1657639
Report Number(s):
IS-J-10,326
Journal ID: ISSN 0034-6748; TRN: US2204193
Grant/Contract Number:  
AC02-07CH11358; GBMF4411; SFB/TR 288
Resource Type:
Accepted Manuscript
Journal Name:
Review of Scientific Instruments
Additional Journal Information:
Journal Volume: 91; Journal Issue: 9; Journal ID: ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)
Country of Publication:
United States
Language:
English
Subject:
47 OTHER INSTRUMENTATION; Measuring instruments; Calibration methods; Electrical properties and parameters; Sensors

Citation Formats

Xiang, Li, Gati, Elena, Bud’ko, Sergey L., Ribeiro, Raquel A., Ata, Arif, Tutsch, Ulrich, Lang, Michael, and Canfield, Paul C. Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells. United States: N. p., 2020. Web. doi:10.1063/5.0022650.
Xiang, Li, Gati, Elena, Bud’ko, Sergey L., Ribeiro, Raquel A., Ata, Arif, Tutsch, Ulrich, Lang, Michael, & Canfield, Paul C. Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells. United States. https://doi.org/10.1063/5.0022650
Xiang, Li, Gati, Elena, Bud’ko, Sergey L., Ribeiro, Raquel A., Ata, Arif, Tutsch, Ulrich, Lang, Michael, and Canfield, Paul C. Thu . "Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells". United States. https://doi.org/10.1063/5.0022650. https://www.osti.gov/servlets/purl/1670358.
@article{osti_1670358,
title = {Characterization of the pressure coefficient of manganin and temperature evolution of pressure in piston-cylinder cells},
author = {Xiang, Li and Gati, Elena and Bud’ko, Sergey L. and Ribeiro, Raquel A. and Ata, Arif and Tutsch, Ulrich and Lang, Michael and Canfield, Paul C.},
abstractNote = {Here, we report measurements of the temperature- and pressure-dependent resistance, R(T, p), of a manganin manometer in a 4He-gas pressure setup from room temperature down to the solidification temperature of 4He (Tsolid ~ 50 K at 0.8 GPa) for pressures, p, between 0 GPa and ~0.8 GPa. The same manganin wire manometer was also measured in a piston-cylinder cell (PCC) from 300 K down to 1.8 K and for pressures between 0 GPa and ~2 GPa. From these data, we infer the temperature and pressure dependence of the pressure coefficient of manganin, α(T, p), defined by the equation Rp = (1 + αp)R0, where R0 and Rp are the resistances of manganin at ambient pressure and finite pressure, respectively. Our results indicate that upon cooling, α first decreases, then goes through a broad minimum at ~120 K, and increases again toward lower temperatures. In addition, we find that α is almost pressure-independent at T ≳ 60 K up to p ~ 2 GPa, but shows a pronounced p dependence at T ≲ 60 K. Using this manganin manometer, we demonstrate that p overall decreases with decreasing temperature in the PCC for the full pressure range and that the size of the pressure difference between room temperature and low temperatures (T = 1.8 K), Δp, decreases with increasing pressure. We also compare the pressure values inferred from the manganin manometer with the low-temperature pressure, determined from the superconducting transition temperature of elemental lead (Pb). As a result of these data and analysis, we propose a practical algorithm to infer the evolution of pressure with temperature in a PCC.},
doi = {10.1063/5.0022650},
journal = {Review of Scientific Instruments},
number = 9,
volume = 91,
place = {United States},
year = {Thu Sep 03 00:00:00 EDT 2020},
month = {Thu Sep 03 00:00:00 EDT 2020}
}

Works referenced in this record:

A diamond anvil cell for the investigation of superconductivity under pressures of up to 50 GPa: Pb as a low temperature manometer
journal, September 1988


Pressure dependence of T c for lead
journal, August 1978

  • Clark, M. J.; Smith, T. F.
  • Journal of Low Temperature Physics, Vol. 32, Issue 3-4
  • DOI: 10.1007/bf00117966

The Curie temperature and the effect of pressure of Ni-based alloys (Ni-Cu, -Pd, -Pt and -Rh)
journal, January 1979


A high pressure bomb for work at low temperatures
journal, December 1964


A method of increasing the hydrostatic nature of the compression at low temperatures in fixed pressure bombs
journal, August 1974


The variation of the pressure coefficient of manganin sensors at low temperatures
journal, January 1999


The Resistance of 72 Elements, Alloys and Compounds to 100,000 Kg/Cm²
journal, January 1952

  • Bridgman, P. W.
  • Proceedings of the American Academy of Arts and Sciences, Vol. 81, Issue 4
  • DOI: 10.2307/20023677

High-resolution thermal expansion measurements under helium-gas pressure
journal, August 2012

  • Manna, Rudra Sekhar; Wolf, Bernd; de Souza, Mariano
  • Review of Scientific Instruments, Vol. 83, Issue 8
  • DOI: 10.1063/1.4747272

Simple clamp pressure cell up to 30 kbar
journal, October 1980

  • Fujiwara, Hiroshi; Kadomatsu, Hideoki; Tohma, Kiyokazu
  • Review of Scientific Instruments, Vol. 51, Issue 10
  • DOI: 10.1063/1.1136061

An Optical Fluorescence System for Quantitative Pressure Measurement in the Diamond‐Anvil Cell
journal, January 1973

  • Barnett, J. D.; Block, S.; Piermarini, G. J.
  • Review of Scientific Instruments, Vol. 44, Issue 1
  • DOI: 10.1063/1.1685943

Pressure Measurement Made by the Utilization of Ruby Sharp-Line Luminescence
journal, April 1972


The Measurement of Hydrostatic Pressures up to 20,000 Kilograms per Square Centimeter
journal, January 1911

  • Bridgman, P. W.
  • Proceedings of the American Academy of Arts and Sciences, Vol. 47, Issue 11
  • DOI: 10.2307/20022746

Superconducting manometers for high pressure measurement at low temperature
journal, February 1969


Pressure-induced multiple phase transformations of the BaBi 3 superconductor
journal, December 2018


Fabrication and efficiency evaluation of a hybrid NiCrAl pressure cell up to 4GPa
journal, July 2007

  • Fujiwara, Naoki; Matsumoto, Takehiko; Nakazawab, Kazuko-
  • Review of Scientific Instruments, Vol. 78, Issue 7
  • DOI: 10.1063/1.2757129

Comparison of pressures at 300 K and liquid helium temperatures using a clamp‐type bomb
journal, May 1976

  • Becker, W. M.; Hoo, Kuong; Winchell, P. G.
  • Review of Scientific Instruments, Vol. 47, Issue 5
  • DOI: 10.1063/1.1134693

Investigation of a strong titanium alloy KS15-5-3 and the application to a high pressure apparatus for magnetization measurements
journal, January 2001

  • Kamishima, K.; Hagiwara, M.; Yoshida, H.
  • Review of Scientific Instruments, Vol. 72, Issue 2
  • DOI: 10.1063/1.1337074

Toward an internally consistent pressure scale
journal, May 2007

  • Fei, Y.; Ricolleau, A.; Frank, M.
  • Proceedings of the National Academy of Sciences, Vol. 104, Issue 22
  • DOI: 10.1073/pnas.0609013104

Measurements of elastoresistance under pressure by combining in-situ tunable quasi-uniaxial stress with hydrostatic pressure
journal, February 2020

  • Gati, Elena; Xiang, Li; Bud’ko, Sergey L.
  • Review of Scientific Instruments, Vol. 91, Issue 2
  • DOI: 10.1063/1.5139437

Simple adaptation of the Bridgman high pressure technique for use with liquid media
journal, September 2007

  • Colombier, E.; Braithwaite, D.
  • Review of Scientific Instruments, Vol. 78, Issue 9
  • DOI: 10.1063/1.2778629

Pressure Calibration to 60 kbar Based on the Resistance Change of a Manganin Coil under Hydrostatic Pressure
journal, April 1969

  • Zeto, Robert J.; Vanfleet, H. B.
  • Journal of Applied Physics, Vol. 40, Issue 5
  • DOI: 10.1063/1.1657962

Solidification of helium, at room temperature under high pressure
journal, January 1979


Electrical Resistance of Manganin Coil to 7 kbar and 200°C
journal, January 1967

  • Wang, Chi‐yuen
  • Review of Scientific Instruments, Vol. 38, Issue 1
  • DOI: 10.1063/1.1720520

Recent advances in high-pressure science and technology
journal, January 2016


Electrical resistance of Manganin under high static pressures
journal, September 1978

  • Fujioka, N.; Mishima, O.; Endo, S.
  • Journal of Applied Physics, Vol. 49, Issue 9
  • DOI: 10.1063/1.325512

Adaptation of the Bridgman anvil cell to liquid pressure mediums
journal, December 2007

  • Rüetschi, A. -S.; Jaccard, D.
  • Review of Scientific Instruments, Vol. 78, Issue 12
  • DOI: 10.1063/1.2818788

The Kondo lattice and weak antiferromagnetism
journal, July 1977


Pressure as a parameter in the study of dilute magnetic alloys
journal, October 1979


Conventional superconductivity at 203 kelvin at high pressures in the sulfur hydride system
journal, August 2015

  • Drozdov, A. P.; Eremets, M. I.; Troyan, I. A.
  • Nature, Vol. 525, Issue 7567
  • DOI: 10.1038/nature14964

Hydrostatic and Uniaxial Pressure Generation using Teflon Cell Container in Conventional Piston‐Cylinder Device
journal, January 1967

  • Jayaraman, A.; Hutson, A. R.; McFee, J. H.
  • Review of Scientific Instruments, Vol. 38, Issue 1
  • DOI: 10.1063/1.1720527

High pressure studies on Fe-pnictide superconductors
journal, May 2009


Calibration of the pressure dependence of the R 1 ruby fluorescence line to 195 kbar
journal, June 1975

  • Piermarini, G. J.; Block, S.; Barnett, J. D.
  • Journal of Applied Physics, Vol. 46, Issue 6
  • DOI: 10.1063/1.321957

Low temperature calibration of Manganin pressure gauges
journal, February 1997

  • Andersson, O. E.; Sundqvist, B.
  • Review of Scientific Instruments, Vol. 68, Issue 2
  • DOI: 10.1063/1.1147868

High-temperature superconductivity in iron-based materials
journal, August 2010

  • Paglione, Johnpierre; Greene, Richard L.
  • Nature Physics, Vol. 6, Issue 9
  • DOI: 10.1038/nphys1759

Foundations of heavy-fermion superconductivity: lattice Kondo effect and Mott physics
journal, July 2016


Use of Cernox thermometers in AC specific heat measurements under pressure
journal, February 2019

  • Gati, Elena; Drachuck, Gil; Xiang, Li
  • Review of Scientific Instruments, Vol. 90, Issue 2
  • DOI: 10.1063/1.5084730

Solidification and loss of hydrostaticity in liquid media used for pressure measurements
journal, December 2015

  • Torikachvili, M. S.; Kim, S. K.; Colombier, E.
  • Review of Scientific Instruments, Vol. 86, Issue 12
  • DOI: 10.1063/1.4937478

X‐Ray Diffraction Studies in the 100 Kilobar Pressure Range
journal, March 1962

  • Jamieson, John C.; Lawson, A. W.
  • Journal of Applied Physics, Vol. 33, Issue 3
  • DOI: 10.1063/1.1777167

Low‐temperature pressure variations in a self‐clamping pressure cell
journal, February 1984

  • Thompson, J. D.
  • Review of Scientific Instruments, Vol. 55, Issue 2
  • DOI: 10.1063/1.1137730

Linear thermal expansivity (1.5–300 K) and heat capacity (1.2–90 K) of Stycast 2850FT
journal, February 1997

  • Swenson, C. A.
  • Review of Scientific Instruments, Vol. 68, Issue 2
  • DOI: 10.1063/1.1148064

A neutron diffraction investigation of Au2Mn under pressure
journal, June 1966

  • Smith, F. A.; Bradley, C. C.; Bacon, G. E.
  • Journal of Physics and Chemistry of Solids, Vol. 27, Issue 6-7
  • DOI: 10.1016/0022-3697(66)90063-1