Mechanical properties and microstructural characteristics of laser and electron-beam welds in V-4Cr-4Ti.
Mechanical properties and microstructural characteristics of laser and electron-beam welds of a 500-kg heat of V4Cr4Ti were investigated in as-welded condition and after postwelding heat treatment by impact testing, microhardness measurement, optical microscopy, X-ray diffraction, and transmission electron microscopy (TEM). Ductile-brittle transition temperatures of the laser and electron-beam welds were significantly higher than that of the base metal. However, excellent impact properties could be restored in both types of welds by postwelding annealing at 1000 C for 1 h in vacuum. Analysis by TEM revealed that annealed weld zones were characterized by extensive networks of fine V(C,O,N) precipitates, which clean away O, C, and N interstitial from the grain matrices. This process is accompanied by simultaneous annealing-out of the dense dislocations present in the weld zone. This finding could be useful in identifying an optimal welding procedure by controlling and adjusting the cooling rate of the weld zone by an innovative method to maximize the precipitation of V(C,O,N).
- Research Organization:
- Argonne National Lab., IL (US)
- Sponsoring Organization:
- US Department of Energy (US)
- DOE Contract Number:
- W-31109-ENG-38
- OSTI ID:
- 10797
- Report Number(s):
- ANL/ET/CP-96421; TRN: AH200127%%413
- Resource Relation:
- Conference: 8th International Conference on Fusion Reactor Materials, Sendai (JP), 10/26/1997--10/31/1997; Other Information: PBD: 18 May 1998
- Country of Publication:
- United States
- Language:
- English
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