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Title: Preparation of carbon nanoparticles and carbon nitride from high nitrogen compound

Patent ·
OSTI ID:988846

The high-nitrogen compound 3,6-di(azido)-1,2,4,5-tetrazine (DiAT) was synthesized by a relatively simple method and used as a precursor for the preparation of carbon nanospheres and nanopolygons, and nitrogen-rich carbon nitrides.

Research Organization:
Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
W-7405-ENG-36
Assignee:
Los Almos National Security, LLC (Los Alamos, NM)
Patent Number(s):
7,582,273
Application Number:
11/257,546
OSTI ID:
988846
Country of Publication:
United States
Language:
English

References (17)

Synthesis, Characterization, and Energetic Properties of Diazido Heteroaromatic High-Nitrogen C−N Compound journal September 2005
A review of investigations on biocompatibility of diamond-like carbon and carbon nitride films journal September 2000
Synthesis of the bi-heterocyclic parent ring system 1,2,4-triazolo[4,3- b ][1,2,4,5]tetrazine and some 3,6-disubstituted derivatives journal November 1998
Polyazido High-Nitrogen Compounds: Hydrazo- and Azo-1,3,5-triazine journal September 2004
Synthesis and Structure of 2,5,8-Triazido- s -Heptazine:  An Energetic and Luminescent Precursor to Nitrogen-Rich Carbon Nitrides journal May 2004
On Accretion of Nanosize Carbon Spheres journal January 1996
Characteristics of meso-carbon microbeads separated from pitch journal June 1974
Synthesis of Nitrogen-Rich Carbon Nitride Networks from an Energetic Molecular Azide Precursor journal December 2000
Texture and graphitization behaviour of fluid coke journal December 1974
An improved synthesis of 3,6-diamino-1,2,4,5-tetrazine. II. From triaminoguanidine and 2,4-pentanedione journal December 1991
3,6-Di(azido)-1,2,4,5-Tetrazine: A Precursor for the Preparation of Carbon Nanospheres and Nitrogen-Rich Carbon Nitrides journal October 2004
Recent progress in the synthesis and characterization of amorphous and crystalline carbon nitride coatings journal January 2000
Mesophase Putch and Meso-Carbon Microbeads journal January 1983
Preparation of microporous carbon nanospheres journal January 2003
The Reaction of Hydrazine with 3,6-Diamino-s-tetrazine 1 journal September 1963
B/C/N Materials Based on the Graphite Network journal July 1997
Synthesis, Characterization, and Explosive Properties of the Nitrogen-Rich Borazine [H 3 N 3 B 3 (N 3 ) 3 ] journal August 1999

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