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Title: Nanometer-scale imaging and pore-scale fluid flow modeling inchalk

Journal Article · · SPE (Society of Petroleum Engineers) Reservoir Evaluation and Engineering
OSTI ID:919756

For many rocks of high economic interest such as chalk,diatomite, tight gas sands or coal, nanometer scale resolution is neededto resolve the 3D-pore structure, which controls the flow and trapping offluids in the rocks. Such resolutions cannot be achieved with existingtomographic technologies. A new 3D imaging method, based on serialsectioning and using the Focused Ion Beam (FIB) technology has beendeveloped. FIB allows for the milling of layers as thin as 10 nanometersby using accelerated Ga+ ions to sputter atoms from the sample surface.After each milling step, as a new surface is exposed, a 2D image of thissurface is generated. Next, the 2D images are stacked to reconstruct the3D pore or grain structure. Resolutions as high as 10 nm are achievableusing this technique. A new image processing method uses directmorphological analysis of the pore space to characterize thepetrophysical properties of diverse formations. In addition to estimationof the petrophysical properties (porosity, permeability, relativepermeability and capillary pressures), the method is used for simulationof fluid displacement processes, such as those encountered in variousimproved oil recovery (IOR) approaches. Computed with the new methodcapillary pressure curves are in good agreement with laboratory data. Themethod has also been applied for visualization of the fluid distributionat various saturations from the new FIB data.

Research Organization:
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
Sponsoring Organization:
USDOE Director. Office of Science. Biological andEnvironmental Research
DOE Contract Number:
DE-AC02-05CH11231
OSTI ID:
919756
Report Number(s):
LBNL-59822; R&D Project: 469501; BnR: KP1201030; TRN: US200822%%520
Journal Information:
SPE (Society of Petroleum Engineers) Reservoir Evaluation and Engineering, Vol. 10, Issue 3; Related Information: Journal Publication Date: 06/2007; ISSN 1094-6470
Country of Publication:
United States
Language:
English