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Title: Condensed phase preparation of 2,3-pentanedione

Patent ·
OSTI ID:871954

A condensed phase process for the preparation of purified 2,3-pentanedione from lactic acid and an alkali metal lactate is described. The process uses elevated temperatures between about 200.degree. to 360.degree. C. for heating a reaction mixture of lactic acid and an alkali metal lactate to produce the 2,3-pentanedione in a reaction vessel. The 2,3-pentanedione produced is vaporized from the reaction vessel and condensed with water.

Research Organization:
The Consortium for Plant Biotechnology Research, Inc., West Lafayette, IN (US)The Consortium for Plant Biotechnology Research, Inc., West Lafayette, IN (US)
DOE Contract Number:
FC05-92OR22072
Assignee:
Board of Trustees operating Michigan State University (East Lansing, MI)
Patent Number(s):
US 5831130
OSTI ID:
871954
Country of Publication:
United States
Language:
English

References (5)

Catalysts and Supports for Conversion of Lactic Acid to Acrylic Acid and 2,3-Pentanedione journal March 1995
FTIR and31P-NMR Spectroscopic Analyses of Surface Species in Phosphate-Catalyzed Lactic Acid Conversion journal November 1996
Formation of 2,3-Pentanedione from Lactic Acid over Supported Phosphate Catalysts journal July 1994
Enhanced activity of in and Ga-supported sol-gel alumina catalysts for NO reduction by hydrocarbons in lean conditions journal February 1998
Lactic Acid Conversion to 2,3-Pentanedione and Acrylic Acid over Silica-Supported Sodium Nitrate: Reaction Optimization and Identification of Sodium Lactate as the Active Catalyst journal January 1997