Method and apparatus for detecting gem-polyhalogenated hydrocarbons
Patent
·
OSTI ID:867413
- (late of Livermore, CA)
- (Palm Springs, CA)
A method and optrode for detecting gem polyhalogenated hydrocarbons in a sample fluid based on a single phase Fujiwara reaction as provided. The method comprises contacting a reaction mixture with a sample fluid which contains the gem-polyhalogenated hydrocarbons. The reaction mixture comprises an aqueous solution of pyridine or derivative thereof and a hindered nitrogen base. Upon contact a fluorescent and/or chromgenic reaction product forms whose fluorescence and/or absorbance is related to the concentration of gem-polyhalogenated hydrocarbons in the sample fluid.
- Research Organization:
- Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
- DOE Contract Number:
- W-7405-ENG-48
- Assignee:
- Regents of University of California (Berkeley, CA)
- Patent Number(s):
- US 4929562
- OSTI ID:
- 867413
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
method
apparatus
detecting
gem-polyhalogenated
hydrocarbons
optrode
gem
polyhalogenated
sample
fluid
based
single
phase
fujiwara
reaction
provided
comprises
contacting
mixture
contains
aqueous
solution
pyridine
derivative
hindered
nitrogen
base
contact
fluorescent
chromgenic
product
forms
fluorescence
absorbance
related
concentration
halogenated hydrocarbons
comprises contacting
method comprises
aqueous solution
reaction mixture
reaction product
sample fluid
single phase
halogenated hydrocarbon
method comprise
mixture comprises
fujiwara reaction
nitrogen base
/436/422/
apparatus
detecting
gem-polyhalogenated
hydrocarbons
optrode
gem
polyhalogenated
sample
fluid
based
single
phase
fujiwara
reaction
provided
comprises
contacting
mixture
contains
aqueous
solution
pyridine
derivative
hindered
nitrogen
base
contact
fluorescent
chromgenic
product
forms
fluorescence
absorbance
related
concentration
halogenated hydrocarbons
comprises contacting
method comprises
aqueous solution
reaction mixture
reaction product
sample fluid
single phase
halogenated hydrocarbon
method comprise
mixture comprises
fujiwara reaction
nitrogen base
/436/422/