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Title: Measuring the Fracture Toughness of TZM and ODS Molybdenum Alloys Using Standard and Sub-Sized Bend Specimens

Technical Report ·
DOI:https://doi.org/10.2172/807260· OSTI ID:807260

Oxide Dispersion Strengthened (ODS) and TZM molybdenum have excellent creep resistance and strength at high temperatures in inert atmospheres. Fracture toughness and tensile testing was performed at temperatures between -150 degrees C and 450 degrees C to characterize 6.35 mm thick plate material of ODS and TZM molybdenum. A transition from low fracture toughness values (5.8 to 29.6 MPa square root m) to values greater than 30 MPa square root m is observed for TZM molybdenum in the longitudinal orientation at 100 degrees C and in the transverse orientation at 150 degrees C. These results are consistent with data reported in literature for molybdenum. A transition to low fracture toughness values (less than 30 MPa square root m) was not observed for longitudinal ODS molybdenum at temperatures greater than or equal to -150 degrees C, while a transition to low fracture toughness values (12.6 to 25.4 MPa square root m) was observed for the transverse orientation at room-temperature. The fi ne spacing of La-oxide precipitates that are present in ODS molybdenum result in a transition temperature that is significantly lower than any molybdenum alloy reported to date, with upper bound fracture toughness values that bound the literature data. A comparison of fracture toughness values obtained using a 1T, 0.5T, and 0.25T Charpy shows that a 0.5T Charpy could be used as a sub-sized specimen geometry.

Research Organization:
Bettis Atomic Power Lab., West Mifflin, PA (US)
Sponsoring Organization:
US Department of Energy (US)
DOE Contract Number:
AC11-98PN38206
OSTI ID:
807260
Report Number(s):
B-T-3387; TRN: US200411%%633
Resource Relation:
Other Information: Supercedes report DE00807260; PBD: 1 Dec 2002; PBD: 1 Dec 2002
Country of Publication:
United States
Language:
English