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Title: Compositions and methods for the dissolution and depolymerization of lignin

Patent ·
OSTI ID:1734997

The present invention provides for a method for dissolving and/or depolymerizing lignin comprising: (a) providing a composition comprising lignin, (b) contacting the composition with a strong hydrogen donor, such as a polyol, to form a first solution, (c) incubating the first solution at a temperature equal to or less than 100° C., whereby at least 20% by weight of the lignin is dissolved, (d) optionally introducing an oxidation agent to the first solution to form a second solution, wherein the temperature of the second solution is equal to or less than 100° C., whereby lignin is depolymerized, and (e) optionally introducing an anti-solvent to the second solution to precipitate the depolymerized lignin.

Research Organization:
Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC02-05CH11231
Assignee:
National Technology & Engineering Solutions of Sandia, LLC (Albuquerque, NM)
Patent Number(s):
10,703,770
Application Number:
15/615,777
OSTI ID:
1734997
Resource Relation:
Patent File Date: 06/06/2017
Country of Publication:
United States
Language:
English

References (3)

Metal Catalyzed Oxidation of Lignin and Related Compounds patent-application September 2014
Method of Treating Plant Biomass patent-application May 2013
Methods and systems for processing lignin during hydrothermal digestion of cellulosic biomass solids patent February 2017