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Title: Experimental issues in in-situ synchrotron x-ray diffraction at high pressure and temperature by using a laser-heated diamond-anvil cell

Abstract

An integrated technique of diamond-anvil cell, laser-heating and synchrotron x-ray diffraction technologies is capable of structural investigation of condensed matter in an extended region of high pressures and temperatures above 100 GPa and 3000 K. The feasibility of this technique to obtain reliable data, however, strongly depends on several experimental issues, including optical and x-ray setups, thermal gradients, pressure homogeneity, preferred orientation, and chemical reaction. In this paper, we discuss about these experimental issues together with future perspectives of this technique for obtaining accurate data.

Authors:
Publication Date:
Research Org.:
Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
Sponsoring Org.:
USDOE, Washington, DC (US)
OSTI Identifier:
16595
Report Number(s):
UCRL-JC-129176; CONF-971201-
ON: DE98054340; BR: DP0102012; TRN: US0205290
DOE Contract Number:  
W-7405-Eng-48
Resource Type:
Conference
Resource Relation:
Conference: Conference title not supplied, Conference location not supplied, Conference dates not supplied; Other Information: Supercedes report DE98054340; PBD: 1 Dec 1997; PBD: 1 Dec 1997
Country of Publication:
United States
Language:
English
Subject:
02 PETROLEUM; 43 PARTICLE ACCELERATORS; CHEMICAL REACTIONS; GRAIN ORIENTATION; SYNCHROTRONS; TEMPERATURE GRADIENTS; X-RAY DIFFRACTION

Citation Formats

Yoo, C S. Experimental issues in in-situ synchrotron x-ray diffraction at high pressure and temperature by using a laser-heated diamond-anvil cell. United States: N. p., 1997. Web.
Yoo, C S. Experimental issues in in-situ synchrotron x-ray diffraction at high pressure and temperature by using a laser-heated diamond-anvil cell. United States.
Yoo, C S. 1997. "Experimental issues in in-situ synchrotron x-ray diffraction at high pressure and temperature by using a laser-heated diamond-anvil cell". United States. https://www.osti.gov/servlets/purl/16595.
@article{osti_16595,
title = {Experimental issues in in-situ synchrotron x-ray diffraction at high pressure and temperature by using a laser-heated diamond-anvil cell},
author = {Yoo, C S},
abstractNote = {An integrated technique of diamond-anvil cell, laser-heating and synchrotron x-ray diffraction technologies is capable of structural investigation of condensed matter in an extended region of high pressures and temperatures above 100 GPa and 3000 K. The feasibility of this technique to obtain reliable data, however, strongly depends on several experimental issues, including optical and x-ray setups, thermal gradients, pressure homogeneity, preferred orientation, and chemical reaction. In this paper, we discuss about these experimental issues together with future perspectives of this technique for obtaining accurate data.},
doi = {},
url = {https://www.osti.gov/biblio/16595}, journal = {},
number = ,
volume = ,
place = {United States},
year = {Mon Dec 01 00:00:00 EST 1997},
month = {Mon Dec 01 00:00:00 EST 1997}
}

Conference:
Other availability
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