Processing of Dilute Mg–Zn–Mn–Ca Alloy/Nb Multilayers by Accumulative Roll Bonding

Leu, Brandon; Savage, Daniel J; Wang, Jiaxiang; Alam, Md Ershadul; Mara, Nathan A; Mariyappan, Arul Kumar; Carpenter, John S.; Vogel, Sven C.; Knezevic, Marko; Decker, Ray; Beyerlein, Irene

doi:10.1002/adem.201900673

Title: Processing of Dilute Mg–Zn–Mn–Ca Alloy/Nb Multilayers by Accumulative Roll Bonding

Journal Article · Tue Jul 23 00:00:00 EDT 2019 · Advanced Engineering Materials

DOI:https://doi.org/10.1002/adem.201900673· OSTI ID:1566117

Leu, Brandon ^[1]; Savage, Daniel J ^[2]; Wang, Jiaxiang ^[1]; Alam, Md Ershadul ^[1]; Mara, Nathan A ^[3];

^[4];

^[4]; Knezevic, Marko ^[2]; Decker, Ray ^[5]; Beyerlein, Irene ^[1]

Univ. of California, Santa Barbara, CA (United States). Dept. of Materials Engineering
Univ. of New Hampshire, Durham, NH (United States). College of Engineering and Physical Sciences
Univ. of Minnesota, Minneapolis, MN (United States). Dept. of Chemical Engineering and Materials Science
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
nanoMAG LLC, Livonia, MI (United States)

Recent advancements in the severe plastic deformation process called accumulative roll bonding (ARB) can help to address the long‐standing need for manufacturing lightweight, high‐strength Mg sheet materials. However, the fabrication of Mg alloy‐based laminates via ARB remains a challenge due to the intrinsically poor formability of Mg. Herein, it is shown that Mg‐based composite laminates with refined layers can be fabricated via several room‐temperature ARB cycles with appropriate intermediate annealing and alloy selection. The final laminates made here consist of equal volume fractions of a dilute Mg–Zn–Mn–Ca alloy phase and a pure Nb phase with fine 150 μm layer thicknesses. Deformation texture evolution in both phases within the composite is analyzed via neutron diffraction measurements taken at different stages in the process. The analysis suggests that the annealing step recrystallizes the Mg‐alloy phase. It is also shown that for both phases, the stabilized deformation textures within the composite correspond to the classic stable textures of the individual constituents. Polycrystal texture modeling implies that {10–12} <‐1011> extension twinning developed in the Mg alloy during rolling.

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Research Organization:: Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)

Sponsoring Organization:: USDOE Office of Science (SC). Basic Energy Sciences (BES) (SC-22); USDOE

Grant/Contract Number:: 89233218CNA000001; FWP 06SCPE401

OSTI ID:: 1566117

Alternate ID(s):: OSTI ID: 1558817

Report Number(s):: LA-UR-19-25330

Journal Information:: Advanced Engineering Materials, Vol. 22, Issue 1; ISSN 1438-1656

Publisher:: WileyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 11 works

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References (62)

Bulk texture evolution of Cu–Nb nanolamellar composites during accumulative roll bonding Carpenter, J. S.; Vogel, S. C.; LeDonne, J. E. Acta Materialia, Vol. 60, Issue 4 https://doi.org/10.1016/j.actamat.2011.11.045	journal	February 2012
Effect of microstructure on the nucleation of deformation twins in polycrystalline high-purity magnesium: A multi-scale modeling study Beyerlein, I. J.; McCabe, R. J.; Tomé, C. N. Journal of the Mechanics and Physics of Solids, Vol. 59, Issue 5 https://doi.org/10.1016/j.jmps.2011.02.007	journal	May 2011
The heterophase interface character distribution of physical vapor-deposited and accumulative roll-bonded Cu–Nb multilayer composites Lee, S. -B.; LeDonne, J. E.; Lim, S. C. V. Acta Materialia, Vol. 60, Issue 4 https://doi.org/10.1016/j.actamat.2011.12.007	journal	February 2012
Texture evolution in two-phase Zr/Nb lamellar composites during accumulative roll bonding Knezevic, Marko; Nizolek, Thomas; Ardeljan, Milan International Journal of Plasticity, Vol. 57 https://doi.org/10.1016/j.ijplas.2014.01.008	journal	June 2014
Enhanced Plasticity via Kinking in Cubic Metallic Nanolaminates: Enhanced Plasticity via Kinking in Cubic Metallic Nanolaminates Nizolek, Thomas; Mara, Nathan A.; Beyerlein, Irene J. Advanced Engineering Materials, Vol. 17, Issue 6 https://doi.org/10.1002/adem.201400324	journal	October 2014
Microstructures and Mechanical Properties of Al/Mg Alloy Multilayered Composites Produced by Accumulative Roll Bonding Liu, H. S.; Zhang, B.; Zhang, G. P. Journal of Materials Science & Technology, Vol. 27, Issue 1 https://doi.org/10.1016/S1005-0302(11)60019-4	journal	January 2011
Influence of texture on dynamic recrystallization and deformation mechanisms in rolled or ECAPed AZ31 magnesium alloy del Valle, J. A.; Ruano, O. A. Materials Science and Engineering: A, Vol. 487, Issue 1-2 https://doi.org/10.1016/j.msea.2007.11.024	journal	July 2008
Bulk mechanical alloying of Cu–Ag and Cu/Zr two-phase microstructures by accumulative roll-bonding process Ohsaki, S.; Kato, S.; Tsuji, N. Acta Materialia, Vol. 55, Issue 8 https://doi.org/10.1016/j.actamat.2006.12.027	journal	May 2007
A self-consistent viscoplastic model: prediction of rolling textures of anisotropic polycrystals Lebensohn, R. A.; Tomé, C. N. Materials Science and Engineering: A, Vol. 175, Issue 1-2 https://doi.org/10.1016/0921-5093(94)91047-2	journal	February 1994
Stochastic modeling of twin nucleation in polycrystals: An application in hexagonal close-packed metals Niezgoda, Stephen R.; Kanjarla, Anand K.; Beyerlein, Irene J. International Journal of Plasticity, Vol. 56 https://doi.org/10.1016/j.ijplas.2013.11.005	journal	May 2014
Engineering Interface Structures and Thermal Stabilities via SPD Processing in Bulk Nanostructured Metals Zheng, Shijian; Carpenter, John S.; McCabe, Rodney J. Scientific Reports, Vol. 4, Issue 1 https://doi.org/10.1038/srep04226	journal	February 2014
Interface-dominant multilayers fabricated by severe plastic deformation: Stability under extreme conditions Mara, Nathan A.; Beyerlein, Irene J. Current Opinion in Solid State and Materials Science, Vol. 19, Issue 5 https://doi.org/10.1016/j.cossms.2015.04.002	journal	October 2015
The effect of composition profile shape on the strength of metallic multilayer structures Krzanowski, James E. Scripta Metallurgica et Materialia, Vol. 25, Issue 6 https://doi.org/10.1016/0956-716X(91)90434-3	journal	June 1991
Texture Development in Pure Mg and Mg Alloy AZ31 Gottstein, Günter; Al Samman, T. Materials Science Forum, Vol. 495-497 https://doi.org/10.4028/www.scientific.net/MSF.495-497.623	journal	September 2005
Direct Observations of Confined Layer Slip in Cu/Nb Multilayers Li, Nan; Wang, Jian; Misra, Amit Microscopy and Microanalysis, Vol. 18, Issue 5 https://doi.org/10.1017/S143192761200133X	journal	October 2012
Texture evolution during annealing of magnesium AZ31 alloy Pérez-Prado, M. T.; Ruano, O. A. Scripta Materialia, Vol. 46, Issue 2 https://doi.org/10.1016/S1359-6462(01)01212-X	journal	January 2002
Role of interface structure on the plastic response of Cu/Nb nanolaminates under shock compression: Non-equilibrium molecular dynamics simulations Zhang, R. F.; Germann, T. C.; Wang, J. Scripta Materialia, Vol. 68, Issue 2 https://doi.org/10.1016/j.scriptamat.2012.09.022	journal	January 2013
The effects of texture and extension twinning on the low-cycle fatigue behavior of a rolled magnesium alloy, AZ31B Wu, L.; Agnew, S. R.; Ren, Y. Materials Science and Engineering: A, Vol. 527, Issue 26 https://doi.org/10.1016/j.msea.2010.07.047	journal	October 2010
On the texture evolution of Mg–Zn–Ca alloy with different hot rolling paths Li, Q.; Huang, G. J.; Huang, X. D. Journal of Magnesium and Alloys, Vol. 5, Issue 2 https://doi.org/10.1016/j.jma.2017.06.001	journal	June 2017
Microstructure and mechanical properties of the Mg/Al laminated composite fabricated by accumulative roll bonding (ARB) Wu, K.; Chang, H.; Maawad, E. Materials Science and Engineering: A, Vol. 527, Issue 13-14 https://doi.org/10.1016/j.msea.2010.02.001	journal	May 2010
Cold rolling textures in AZ31 wrought magnesium alloy Styczynski, A.; Hartig, Ch.; Bohlen, J. Scripta Materialia, Vol. 50, Issue 7 https://doi.org/10.1016/j.scriptamat.2004.01.010	journal	April 2004
High strength Mg/Nb nanolayer composites Ham, B.; Zhang, X. Materials Science and Engineering: A, Vol. 528, Issue 4-5 https://doi.org/10.1016/j.msea.2010.10.101	journal	February 2011
Weight Loss with Magnesium Alloys Pollock, T. M. Science, Vol. 328, Issue 5981 https://doi.org/10.1126/science.1182848	journal	May 2010
Dynamic recrystallization of Mg and Mg–Y alloys: Crystallographic texture development Cottam, R.; Robson, J.; Lorimer, G. Materials Science and Engineering: A, Vol. 485, Issue 1-2 https://doi.org/10.1016/j.msea.2007.08.016	journal	June 2008
Dislocation-Based Deformation Mechanisms in Metallic Nanolaminates Anderson, P. M.; Foecke, T.; Hazzledine, P. M. MRS Bulletin, Vol. 24, Issue 2 https://doi.org/10.1557/S0883769400051514	journal	February 1999
Mechanistic origin and prediction of enhanced ductility in magnesium alloys Wu, Zhaoxuan; Ahmad, Rasool; Yin, Binglun Science, Vol. 359, Issue 6374 https://doi.org/10.1126/science.aap8716	journal	January 2018
Texture analysis in hexagonal materials Wang, Y. N.; Huang, J. C. Materials Chemistry and Physics, Vol. 81, Issue 1 https://doi.org/10.1016/S0254-0584(03)00168-8	journal	July 2003
Length-scale-dependent deformation mechanisms in incoherent metallic multilayered composites Misra, A.; Hirth, J. P.; Hoagland, R. G. Acta Materialia, Vol. 53, Issue 18 https://doi.org/10.1016/j.actamat.2005.06.025	journal	October 2005
Processing and Deformation Behavior of Bulk Cu–Nb Nanolaminates Nizolek, T.; Mara, N. A.; Beyerlein, I. J. Metallography, Microstructure, and Analysis, Vol. 3, Issue 6 https://doi.org/10.1007/s13632-014-0172-2	journal	November 2014
Effect of deformation twinning on crystallographic texture evolution in a Mg–6.6Zn–0.2Ca (ZX70) alloy during recrystallisation Guan, Dikai; Liu, Xingguang; Gao, Junheng Journal of Alloys and Compounds, Vol. 774 https://doi.org/10.1016/j.jallcom.2018.10.065	journal	February 2019
Deformation microstructures and textures of some cold rolled Mg alloys Barnett, M. R.; Nave, M. D.; Bettles, C. J. Materials Science and Engineering: A, Vol. 386, Issue 1-2 https://doi.org/10.1016/j.msea.2004.07.030	journal	November 2004
Texture analysis with the new HIPPO TOF diffractometer Wenk, H. -R.; Lutterotti, L.; Vogel, S. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 515, Issue 3 https://doi.org/10.1016/j.nima.2003.05.001	journal	December 2003
Plastic instability mechanisms in bimetallic nanolayered composites Zheng, S. J.; Wang, J.; Carpenter, J. S. Acta Materialia, Vol. 79 https://doi.org/10.1016/j.actamat.2014.07.017	journal	October 2014
Rolling and Recrystallization Textures of BCC Steels Lücke, K.; Hölscher, M. Textures and Microstructures, Vol. 14 https://doi.org/10.1155/TSM.14-18.585	journal	January 1991
A model of continuous dynamic recrystallization Gourdet, S.; Montheillet, F. Acta Materialia, Vol. 51, Issue 9 https://doi.org/10.1016/S1359-6454(03)00078-8	journal	May 2003
Metal-matrix nanocomposites under compressive loading: Towards an understanding of how twinning formation can enhance their plastic deformation Kardani, A.; Montazeri, A. Scientific Reports, Vol. 10, Issue 1 https://doi.org/10.1038/s41598-020-66696-1	journal	June 2020
Texture Evolution in Mg-Zn-Ca Alloy Sheets Kim, D. -W.; Suh, B. -C.; Shim, M. -S. Metallurgical and Materials Transactions A, Vol. 44, Issue 7 https://doi.org/10.1007/s11661-013-1674-2	journal	March 2013
Structure–Property–Functionality of Bimetal Interfaces Beyerlein, I. J.; Mara, N. A.; Wang, J. JOM, Vol. 64, Issue 10 https://doi.org/10.1007/s11837-012-0431-0	journal	September 2012
Modelling discontinuous dynamic recrystallization using a physically based model for nucleation Cram, D. G.; Zurob, H. S.; Brechet, Y. J. M. Acta Materialia, Vol. 57, Issue 17 https://doi.org/10.1016/j.actamat.2009.07.024	journal	October 2009
Determination of pole figure coverage for texture measurements with neutron time-of-flight diffractometers Takajo, Shigehiro; Vogel, Sven C. Journal of Applied Crystallography, Vol. 51, Issue 3 https://doi.org/10.1107/S1600576718007732	journal	June 2018
A six-axis robotic sample changer for high-throughput neutron powder diffraction and texture measurements Losko, Adrian S.; Vogel, Sven C.; Reiche, H. Matthias Journal of Applied Crystallography, Vol. 47, Issue 6 https://doi.org/10.1107/S1600576714021797	journal	November 2014
Bulk texture evolution of nanolamellar Zr–Nb composites processed via accumulative roll bonding Carpenter, J. S.; Nizolek, T.; McCabe, R. J. Acta Materialia, Vol. 92 https://doi.org/10.1016/j.actamat.2015.03.020	journal	June 2015
Experimentally quantifying critical stresses associated with basal slip and twinning in magnesium using micropillars Liu, Y.; Li, N.; Arul Kumar, M. Acta Materialia, Vol. 135 https://doi.org/10.1016/j.actamat.2017.06.008	journal	August 2017
Interface-driven microstructure development and ultra high strength of bulk nanostructured Cu-Nb multilayers fabricated by severe plastic deformation Beyerlein, Irene J.; Mara, Nathan A.; Carpenter, John S. Journal of Materials Research, Vol. 28, Issue 13 https://doi.org/10.1557/jmr.2013.21	journal	April 2013
Review: effect of bimetal interface structure on the mechanical behavior of Cu–Nb fcc–bcc nanolayered composites Mara, Nathan A.; Beyerlein, Irene J. Journal of Materials Science, Vol. 49, Issue 19 https://doi.org/10.1007/s10853-014-8342-9	journal	July 2014
Reduction in Planar Anisotropy of Pure Niobium Sheet by Asymmetric Rolling Ito, Akira; Zhou, Zijian; Utsunomiya, Hiroshi Tetsu-to-Hagane, Vol. 97, Issue 11 https://doi.org/10.2355/tetsutohagane.97.572	journal	January 2011
Texture evolution during large-strain hot rolling of the Mg AZ61 alloy del Valle, J. A.; Pérez-Prado, M. T.; Ruano, O. A. Materials Science and Engineering: A, Vol. 355, Issue 1-2 https://doi.org/10.1016/S0921-5093(03)00043-1	journal	August 2003
Strength and ductility of bulk Cu/Nb nanolaminates exposed to extremely high temperatures Yang, Wenfan; Beyerlein, Irene J.; Jin, Qianqian Scripta Materialia, Vol. 166 https://doi.org/10.1016/j.scriptamat.2019.03.007	journal	June 2019
Cold rolling evolution in high purity niobium using a tapered wedge specimen Jiang, H.; Bieler, T. R.; Compton, C. Physica C: Superconductivity, Vol. 441, Issue 1-2 https://doi.org/10.1016/j.physc.2006.03.025	journal	July 2006
Relationship between texture and low temperature superplasticity in an extruded AZ31 Mg alloy processed by ECAP Lin, H. K.; Huang, J. C.; Langdon, T. G. Materials Science and Engineering: A, Vol. 402, Issue 1-2 https://doi.org/10.1016/j.msea.2005.04.018	journal	August 2005
The texture and anisotropy of magnesium–zinc–rare earth alloy sheets Bohlen, Jan; Nürnberg, Marcus R.; Senn, Jeremy W. Acta Materialia, Vol. 55, Issue 6 https://doi.org/10.1016/j.actamat.2006.11.013	journal	April 2007
Triggering rare earth texture modification in magnesium alloys by addition of zinc and zirconium Basu, I.; Al-Samman, T. Acta Materialia, Vol. 67 https://doi.org/10.1016/j.actamat.2013.12.015	journal	April 2014
Deformation Behavior of Nanostructured Metallic Multilayers Misra, A.; Krug, H. Advanced Engineering Materials, Vol. 3, Issue 4 https://doi.org/10.1002/1527-2648(200104)3:4<217::AID-ADEM217>3.0.CO;2-5	journal	April 2001
Improving the mechanical properties of magnesium and a magnesium alloy through severe plastic deformation Yamashita, Akihiro; Horita, Zenji; Langdon, Terence G. Materials Science and Engineering: A, Vol. 300, Issue 1-2 https://doi.org/10.1016/S0921-5093(00)01660-9	journal	February 2001
Strength and plasticity of nanolaminated materials Wang, Jian; Zhou, Qing; Shao, Shuai Materials Research Letters, Vol. 5, Issue 1 https://doi.org/10.1080/21663831.2016.1225321	journal	July 2016
A dislocation density based crystal plasticity finite element model: Application to a two-phase polycrystalline HCP/BCC composites Ardeljan, Milan; Beyerlein, Irene J.; Knezevic, Marko Journal of the Mechanics and Physics of Solids, Vol. 66 https://doi.org/10.1016/j.jmps.2014.01.006	journal	May 2014
Rietveld texture analysis from TOF neutron diffraction data Wenk, H. -R.; Lutterotti, L.; Vogel, S. C. Powder Diffraction, Vol. 25, Issue 3 https://doi.org/10.1154/1.3479004	journal	September 2010
Forming behavior of magnesium sheet Wagoner, R. H.; Lou, X. Y.; Li, M. Journal of Materials Processing Technology, Vol. 177, Issue 1-3 https://doi.org/10.1016/j.jmatprotec.2006.04.121	journal	July 2006
Atomistic simulations of dislocation–interface interactions in the Cu-Ni multilayer system Rao, S. I.; Hazzledine, P. M. Philosophical Magazine A, Vol. 80, Issue 9 https://doi.org/10.1080/01418610008212148	journal	September 2000
Attempt to Design a Strong Solid Koehler, J. S. Physical Review B, Vol. 2, Issue 2 https://doi.org/10.1103/PhysRevB.2.547	journal	July 1970
A crystal plasticity model for hexagonal close packed (HCP) crystals including twinning and de-twinning mechanisms Wang, H.; Wu, P. D.; Wang, J. International Journal of Plasticity, Vol. 49 https://doi.org/10.1016/j.ijplas.2013.02.016	journal	October 2013
The crystallography and deformation modes of hexagonal close-packed metals Partridge, P. G. International Materials Reviews, Vol. 12, Issue 1 https://doi.org/10.1179/imr.1967.12.1.169	journal	January 1967

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accumulative roll bonding
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Title: Processing of Dilute Mg–Zn–Mn–Ca Alloy/Nb Multilayers by Accumulative Roll Bonding

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