skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Structure/property (constitutive and spallation response) of additively manufactured 316L stainless steel

Journal Article · · Acta Materialia

For additive manufacturing (AM) of metallic materials, the certification and qualification paradigm needs to evolve as there is currently no broadly accepted “ASTM- or DIN-type” additive manufacturing certification process or AM-produced material specifications. Accordingly, design, manufacture, and subsequent implementation and insertion of AM materials to meet engineering applications requires detailed quantification of the constitutive (strength and damage) properties of these evolving materials, across the spectrum of metallic AM methods, in comparison/contrast to conventionally-manufactured metals and alloys. For this paper, cylindrical samples of 316L SS were produced using a LENS MR-7 laser additive manufacturing system from Optomec (Albuquerque, NM) equipped with a 1 kW Yb-fiber laser. The microstructure of the AM-316L SS was characterized in both the “as-built” AM state and following a heat-treatment designed to obtain full recrystallization to facilitate comparison with annealed wrought 316L SS. The constitutive behavior as a function of strain rate and temperature was characterized and is compared to that of annealed wrought 316L SS plate material. The dynamic shock-loading-induced damage evolution and failure response of all three 316L SS materials was quantified using flyer-plate impact driven spallation experiments at peak stresses of 4.7 and 6.5 GPa. The spall strength of AM-produced 316L SS and the recrystallized-AM-316L SS were found to decrease with increasing peak shock stress while the annealed wrought 316L SS spall strength remained essentially constant. Finally, the damage evolution, characterized using optical metallography and electron-backscatter diffraction (EBSD), was found to vary significantly across the three 316L SS microstructures while the three samples loaded to a peak shock stress of 6.5 GPa displayed only ~12% differences in spall strength.

Research Organization:
Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA); USDOD
Grant/Contract Number:
AC52-06NA25396
OSTI ID:
1463491
Alternate ID(s):
OSTI ID: 1549633
Report Number(s):
LA-UR-18-21099
Journal Information:
Acta Materialia, Vol. 138; ISSN 1359-6454
Publisher:
ElsevierCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 138 works
Citation information provided by
Web of Science

References (34)

The metallurgy and processing science of metal additive manufacturing journal March 2016
Metal Additive Manufacturing: A Review journal April 2014
A review on 3D micro-additive manufacturing technologies journal November 2012
Overview of Materials Qualification Needs for Metal Additive Manufacturing journal January 2016
Analysis of rapid manufacturing—using layer manufacturing processes for production journal January 2003
Overview of Current Additive Manufacturing Technologies and Selected Applications journal September 2012
Solidification in direct metal deposition by LENS processing journal September 2001
Understanding thermal behavior in the LENS process journal June 1999
Directed light fabrication of a solid metal hemisphere using 5-axis powder deposition journal March 1998
Development of a Near Net Shape Processing Method for Rhenium Using Directed Light Fabrication journal September 1998
Dynamic Mechanical Behavior of Additively Manufactured Ti6Al4V With Controlled Voids journal April 2015
Spall fracture in additive manufactured Ti-6Al-4V journal October 2016
Charpy impact testing of metallic selective laser melting parts journal June 2010
Density and porosity control of sintered 316L stainless steel parts produced by additive manufacturing journal September 2012
Investigation into the effect of process parameters on microstructural and physical properties of 316L stainless steel parts by selective laser melting journal September 2014
An Experimental Investigation into Additive Manufacturing-Induced Residual Stresses in 316L Stainless Steel journal September 2014
The study of the laser parameters and environment variables effect on mechanical properties of high compact parts elaborated by selective laser melting 316L powder journal November 2013
Damage evolution and failure mechanisms in additively manufactured stainless steel journal January 2016
Role of geometry on properties of additively manufactured Ti-6Al-4V structures fabricated using laser based directed energy deposition journal September 2016
Additive manufactured AlSi10Mg samples using Selective Laser Melting (SLM): Microstructure, high cycle fatigue, and fracture behavior journal February 2012
Wire based additive layer manufacturing: Comparison of microstructure and mechanical properties of Ti–6Al–4V components fabricated by laser-beam deposition and shaped metal deposition journal June 2011
High-Strain-Rate Deformation: Mechanical Behavior and Deformation Substructures Induced journal August 2012
Application of a new automatic lattice orientation measurement technique to polycrystalline aluminum journal February 1993
Influence of shock-wave profile shape (triangulai- “Taylor-wave" versus square-topped) on the spallation response of 316L stainless steel journal September 2003
On the influence of loading profile upon the tensile failure of stainless steel journal May 2007
NIH Image to ImageJ: 25 years of image analysis journal June 2012
Compact system for high-speed velocimetry using heterodyne techniques journal August 2006
Accuracy limits and window corrections for photon Doppler velocimetry journal January 2007
Residual stresses in LENS® components using neutron diffraction and contour method journal June 2005
Residual stresses in components formed by the laserengineered net shaping (LENS®) process journal August 2003
On the Hall-Petch relationship and substructural evolution in type 316L stainless steel journal November 1995
Distortion of the Wave Profiles in an Elastoplastic Body upon Spalling journal January 2001
Effects of grain size and boundary structure on the dynamic tensile response of copper journal August 2011
Influence of anisotropy (crystallographic and microstructural) on spallation in Zr, Ta, HY-100 steel, and 1080 eutectoid steel journal January 2010

Cited By (12)

Assumption of Constraining Force to Explain Distortion in Laser Additive Manufacturing journal November 2018
Anomalous Annealing Response of Directed Energy Deposited Type 304L Austenitic Stainless Steel journal January 2018
Printability of 316 stainless steel journal April 2019
Response of solidification cellular structures in additively manufactured 316 stainless steel to heavy ion irradiation: an in situ study journal April 2019
Microstructure and Corrosion Characteristics of Selective Laser-Melted 316L Stainless Steel: The Impact of Process-Induced Porosities journal July 2019
Microstructure, Solidification Texture, and Thermal Stability of 316 L Stainless Steel Manufactured by Laser Powder Bed Fusion journal August 2018
A comparison of adiabatic shear bands in wrought and additively manufactured 316L stainless steel using nanoindentation and electron backscatter diffraction journal September 2019
Influence of plasma sprayed zirconia coating on surface properties of additive manufactured austenitic stainless steel 316 L journal November 2019
Spall fracture in additive manufactured tantalum journal December 2018
Cause of Angular Distortion in Fusion Welding: Asymmetric Cross-Sectional Profile along Thickness journal December 2018
Printability of 316 stainless steel text January 2019
Defect Prevention in Selective Laser Melting Components: Compositional and Process Effects journal November 2019