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Title: In situ observations of cracking in constrained sintering

Journal Article · · Journal of the American Ceramic Society
DOI:https://doi.org/10.1111/jace.15868· OSTI ID:1461936

Abstract In this paper, we examine the long‐standing problem of cracking during constrained sintering of a powder aggregate. Using binder jet 3D printing, we prepare ceramic green bodies in the form of center‐notched panels, then use in situ imaging to observe how cracks nucleate and grow from the notch as the material sinters under restraint. Quantitative image analysis allows us to identify important characteristics of the sinter‐cracking process, indicating a framework for analyzing the problem and developing methods for avoiding it, including representation of sinter‐cracking as a creep crack growth process, use of fracture mechanics parameters to design specimen geometries that do not exceed critical stress intensities, and the possibility of exploiting the inherently ductile nature of sinter‐cracking to mitigate damage.

Research Organization:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Organization:
USDOE Office of Energy Efficiency and Renewable Energy (EERE)
Grant/Contract Number:
AC05-00OR22725
OSTI ID:
1461936
Alternate ID(s):
OSTI ID: 1457594
Journal Information:
Journal of the American Ceramic Society, Vol. 0, Issue 0; ISSN 0002-7820
Publisher:
American Ceramic SocietyCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 3 works
Citation information provided by
Web of Science

References (16)

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Flaw Generation During Constrained Sintering of Metal-Ceramic and Metal-Glass Multilayer Films journal September 1989
Sintering Behavior of Ceramic Films Constrained by a Rigid Substrate journal June 1985
Evolution of Defects During Sintering: Discrete Element Simulations journal July 2009
Mechanics of sintering thin films — II. Cracking due to self-stress journal May 1991
Powder bed binder jet 3D printing of Inconel 718: Densification, microstructural evolution and challenges☆ journal August 2017
Measurement of the Sintering Pressure in Ceramic Films journal April 1988
Processing-Related Fracture Origins: II, Agglomerate Motion and Cracklike Internal Surfaces Caused by Differential Sintering journal June 1983
Application of fracture mechanics to creep crack growth journal September 1974
Crack Growth and Damage in Constrained Sintering Films journal October 1993
Simulations of the influence of rearrangement during sintering journal January 2007
A second report on sintering diagrams journal February 1981
Fiji: an open-source platform for biological-image analysis journal June 2012
Observations and analysis of sintering damage journal July 1989
Densification of powder rings constrained by dense cylindrical cores journal February 1989
Mechanics of sintering thin films — I. Formulation and analytical results journal September 1990

Figures / Tables (9)


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