From Solidification Processing to Microstructure to Mechanical Properties: A Multi-scale X-ray Study of an Al-Cu Alloy Sample

Tourret, D.; Mertens, J. C.  E.; Lieberman, E.; Imhoff, S. D.; Gibbs, J. W.; Henderson, K.; Fezzaa, K.; Deriy, A. L.; Sun, T.; Lebensohn, R. A.; Patterson, B. M.; Clarke, A. J.

doi:10.1007/s11661-017-4302-8

Title: From Solidification Processing to Microstructure to Mechanical Properties: A Multi-scale X-ray Study of an Al-Cu Alloy Sample

Journal Article · Wed Sep 13 00:00:00 EDT 2017 · Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science

DOI:https://doi.org/10.1007/s11661-017-4302-8· OSTI ID:1396122

Tourret, D. ^[1]; Mertens, J. C. E. ^[2]; Lieberman, E. ^[2]; Imhoff, S. D. ^[2]; Gibbs, J. W. ^[2]; Henderson, K. ^[2]; Fezzaa, K. ^[3]; Deriy, A. L. ^[3]; Sun, T. ^[3]; Lebensohn, R. A. ^[2]; Patterson, B. M. ^[2]; Clarke, A. J. ^[4]

Los Alamos National Lab. (LANL), Los Alamos, NM (United States); IMDEA Materials Inst., Getafe (Spain)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Colorado School of Mines, Golden, CO (United States)

We follow an Al-12at.%Cu alloy sample from the liquid state to mechanical failure, using in situ X-ray radiography during directional solidification and tensile testing, as well as three-dimensional computed tomography of the microstructure before and after mechanical testing. The solidification processing stage is simulated with a multi-scale dendritic needle network model, and the micromechanical behavior of the solidified microstructure is simulated using voxelized tomography data and an elasto-viscoplastic fast Fourier transform model. This study demonstrates the feasibility of direct in situ monitoring of a metal alloy microstructure from the liquid processing stage up to its mechanical failure, supported by quantitative simulations of microstructure formation and its mechanical behavior.

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Research Organization:: Los Alamos National Laboratory (LANL), Los Alamos, NM (United States); Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE; USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22). Materials Sciences & Engineering Division

Grant/Contract Number:: AC52-06NA25396; AC02-06CH11357

OSTI ID:: 1396122

Alternate ID(s):: OSTI ID: 1405300

Report Number(s):: LA-UR-17-21649; TRN: US1702390

Journal Information:: Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science, Vol. 48, Issue 11; ISSN 1073-5623

Publisher:: ASM InternationalCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 18 works

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Web of Science

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Microstructure selection in thin-sample directional solidification of an Al-Cu alloy: In situ X-ray imaging and phase-field simulations

Journal Article · Mon May 01 00:00:00 EDT 2017 · Acta Materialia · OSTI ID:1396122

Clarke, A. J.; Tourret, D.; Song, Y.; +5 more

Microstructure selection in thin-sample directional solidification of an Al-Cu alloy: In situ X-ray imaging and phase-field simulations

Journal Article · Mon May 01 00:00:00 EDT 2017 · Acta Materialia · OSTI ID:1396122

Clarke, A. J.; Tourret, D.; Song, Y.; +5 more

In Situ Synchrotron X-ray Study of Ultrasound Cavitation and Its Effect on Solidification Microstructures

Journal Article · Thu Dec 11 00:00:00 EST 2014 · Metallurgical and Materials Transactions. B, Process Metallurgy and Materials Processing Science · OSTI ID:1396122

Mi, Jiawei; Tan, Dongyue; Lee, Tung Lik

Related Subjects

36 MATERIALS SCIENCE
Processing-Microstructure-Properties
Solidification
Mechanical testing
X-ray radiography and tomography
Mechanical Testing
X-ray Radiography
X-ray tomography

Title: From Solidification Processing to Microstructure to Mechanical Properties: A Multi-scale X-ray Study of an Al-Cu Alloy Sample

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