skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: New materials for high-energy-resolution x-ray optics

Journal Article · · MRS Bulletin
DOI:https://doi.org/10.1557/mrs.2017.94· OSTI ID:1373409
 [1];  [2];  [3];  [1];  [4]
  1. Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
  2. Diamond Light Source Ltd. (United Kingdom)
  3. Argonne National Lab. (ANL), Argonne, IL (United States)
  4. RIKEN SPring-8 Center (Japan)

The use of crystals other than silicon for x-ray optics is becoming more common for many challenging experiments such as resonant inelastic x-ray scattering and nuclear resonant scattering. As more—and more specialized—spectrometers become available at many synchrotron radiation facilities, interest in pushing the limits of experimental energy resolution has increased. The potentially large improvements in resolution and efficiency that nonsilicon optics offer are beginning to be realized. Furthermore, this article covers the background and state of the art for nonsilicon crystal optics with a focus on a resolution of 10 meV or better, concentrating on compounds that form trigonal crystals, including sapphire, quartz, and lithium niobate, rather than the more conventional cubic materials, including silicon, diamond, and germanium.

Research Organization:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22), Scientific User Facilities Division
Grant/Contract Number:
AC02-06CH11357
OSTI ID:
1373409
Journal Information:
MRS Bulletin, Vol. 42, Issue 06; ISSN 0883-7694
Publisher:
Materials Research SocietyCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 7 works
Citation information provided by
Web of Science

References (26)

Rocking curve imaging of high quality sapphire crystals in backscattering geometry journal January 2017
Sapphire analyzers for high-resolution X-ray spectroscopy
  • Yavaş, Hasan; Ercan Alp, E.; Sinn, Harald
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 582, Issue 1 https://doi.org/10.1016/j.nima.2007.08.095
journal November 2007
Nuclear resonant forward scattering of synchrotron radiation from 121 Sb at 37.13 keV journal April 2006
Examination of Bragg backscattering from crystalline quartz journal December 2005
Hard-x-ray spectrographs with resolution beyond 100 μ eV journal April 2013
A synchrotron X-ray diffraction study of a small congruent LiNbO 3 crystal: A compatible approach to powder diffraction journal June 2001
Location of Ti Atoms Diffused into Nearly Perfect Crystals of LiNbO 3 : An X-Ray Standing-Wave Study journal February 1994
Nuclear forward and inelastic spectroscopy on 125 Te and Sb 2 125 Te 3 journal September 2010
Relative x-ray collection efficiency, spatial resolution, and spectral resolution of spherically-bent quartz, mica, germanium, and pyrolytic graphite crystals journal September 2014
MERIX—Next generation medium energy resolution inelastic X-ray scattering instrument at the APS journal June 2013
Tracing X-rays through an L-shaped laterally graded multilayer mirror: a synchrotron application journal March 2010
Single-crystal sapphire microstructure for high-resolution synchrotron X-ray monochromators: Single-crystal sapphire microstructure for high-resolution … journal March 2016
Resonant inelastic x-ray scattering studies of elementary excitations journal June 2011
Collimating Montel mirror as part of a multi-crystal analyzer system for resonant inelastic X-ray scattering journal June 2016
Advances in crystal analyzers for inelastic X-ray scattering journal December 2005
Milli-electronvolt monochromatization of hard X-rays with a sapphire backscattering monochromator journal July 2011
Crystals for quartz resonators journal January 1985
Nearly perfect large-area quartz: 4 meV resolution for 10 keV photons over 10 cm 2 journal April 2006
Precise measurement of the lattice parameters of α-Al 2 O 3 in the temperature range 4.5–250 K using the Mössbauer wavelength standard journal July 2003
Spherical analyzers and monochromators for resonant inelastic hard X-ray scattering: a compilation of crystals and reflections journal November 2012
Exact Bragg backscattering of x rays journal March 1998
Resonant inelastic X-ray scattering spectrometer with 25 meV resolution at the Cu K -edge journal June 2015
The sapphire backscattering monochromator at the Dynamics beamline P01 of PETRA III journal February 2016
High-contrast sub-millivolt inelastic X-ray scattering for nano- and mesoscale science journal June 2014
Quality Assessment of Sapphire Wafers for X-Ray Crystal Optics Using White Beam Synchrotron X-Ray Topography journal August 2001
Rocking curve imaging of high quality sapphire crystals in backscattering geometry text January 2017

Cited By (2)

X-ray back-diffraction: can we further increase the energy resolution by tuning the energy slightly below that of exact backscattering? journal October 2019
Performance of quartz- and sapphire-based double-crystal high-resolution (∼10 meV) RIXS monochromators under varying power loads text January 2018