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Title: Dynamic Reflectance of Tin Shocked from Its Beta to BCT Phase

Conference · · AIP Conference Proceedings
DOI:https://doi.org/10.1063/1.4971713· OSTI ID:1240152

Shock-induced phase transitions have historically been inferred by features in loading/unloading velocity wave profiles, which arise due to volume or sound speed differences between phases. In 2010, we used a flash-lampilluminated ultiband reflectometer to demonstrate that iron, tin, cerium, and gallium have measureable reflectance changes at phase boundaries. We have improved upon our prior technique, utilizing an integrating sphere with an internal xenon flash lamp to illuminate a shocked metal beneath a LiF window. The new reflectance system is insensitive to motion, tilt, or curvature and measures the absolute reflectance within five bands centered at 500, 700, 850, 1064, 1300, and 1550 nm. We have made dynamic reflectance measurements of tin samples shocked to pressures above and below the beta-BCT phase transition using a light gas gun. Below the transition, the visible reflectance decreases with pressure. At and above the transition, the visible reflectance increases to values higher than the ambient values. Reflectance can therefore be used to locate the beta-BCT phase transition boundary for tin, independent of the velocity wave profile. Using the reflectance data, we also present experimental estimates of the phase fraction as a function of shock stress.

Research Organization:
Nevada Test Site (NTS), Mercury, NV (United States)
Sponsoring Organization:
USDOE National Nuclear Security Administration (NNSA)
DOE Contract Number:
DE-AC52-06NA25946
OSTI ID:
1240152
Report Number(s):
DOE/NV/25946-2514
Journal Information:
AIP Conference Proceedings, Vol. 1793, Issue 1; Conference: American Physical Society Shock Compression of Condensed Matter Conference Tampa, FL June 14 - 19, 2015 http://www.aps.org/meetings/meeting.cfm?name=SHOCK15
Country of Publication:
United States
Language:
English

References (6)

Reflectance changes during shock-induced phase transformations in metals journal June 2010
Infrared emissivity of tin upon release of a 25 GPa shock into a lithium fluoride window journal November 2011
Release path temperatures of shock-compressed tin from dynamic reflectance and radiance measurements journal August 2013
Shock induced polymorphic transition and melting of tin conference January 2000
Compact system for high-speed velocimetry using heterodyne techniques journal August 2006
Emissivity measurements of shocked tin using a multi-wavelength integrating sphere journal November 2011

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