Quantitative analysis of the local phase transitions induced by the laser heating

Levlev, Anton V.; Susner, Michael A.; McGuire, Michael A.; Maksymovych, Petro; Kalinin, Sergei V.

doi:10.1021/acsnano.5b05818

Title: Quantitative analysis of the local phase transitions induced by the laser heating

Journal Article · Wed Nov 04 00:00:00 EST 2015 · ACS Nano

DOI:https://doi.org/10.1021/acsnano.5b05818· OSTI ID:1237621

Levlev, Anton V. ^[1]; Susner, Michael A. ^[1]; McGuire, Michael A. ^[1]; Maksymovych, Petro ^[1]; Kalinin, Sergei V. ^[1]

Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

Functional imaging enabled by scanning probe microscopy (SPM) allows investigations of nanoscale material properties under a wide range of external conditions, including temperature. However, a number of shortcomings preclude the use of the most common material heating techniques, thereby limiting precise temperature measurements. Here we discuss an approach to local laser heating on the micron scale and its applicability for SPM. In addition, we applied local heating coupled with piezoresponse force microscopy and confocal Raman spectroscopy for nanoscale investigations of a ferroelectric-paraelectric phase transition in the copper indium thiophosphate layered ferroelectric. Bayesian linear unmixing applied to experimental results allowed extraction of the Raman spectra of different material phases and enabled temperature calibration in the heated region. The obtained results enable a systematic approach for studying temperature-dependent material functionalities in heretofore unavailable temperature regimes.

View Accepted Manuscript (DOE)

Cite

Export

Save

Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States). Center for Nanophase Materials Sciences (CNMS)

Sponsoring Organization:: USDOE Office of Science (SC)

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1237621

Alternate ID(s):: OSTI ID: 1265919

Journal Information:: ACS Nano, Vol. 9, Issue 12; ISSN 1936-0851

Publisher:: American Chemical Society (ACS)Copyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 20 works

Citation information provided by
Web of Science

References (46)

Atomic-Force Microscopy Binnig, G. K. Physica Scripta, Vol. T19A https://doi.org/10.1088/0031-8949/1987/T19A/008	journal	January 1987
Imaging spectroscopy with the atomic force microscope Baselt, David R.; Baldeschwieler, John D. Journal of Applied Physics, Vol. 76, Issue 1 https://doi.org/10.1063/1.357150	journal	July 1994
Acoustic microscopy by atomic force microscopy Rabe, U.; Arnold, W. Applied Physics Letters, Vol. 64, Issue 12 https://doi.org/10.1063/1.111869	journal	March 1994
Nanoscale subsurface imaging via resonant difference-frequency atomic force ultrasonic microscopy Cantrell, Sean A.; Cantrell, John H.; Lillehei, Peter T. Journal of Applied Physics, Vol. 101, Issue 11 https://doi.org/10.1063/1.2743908	journal	June 2007
Kelvin probe force microscopy Nonnenmacher, M.; O’Boyle, M. P.; Wickramasinghe, H. K. Applied Physics Letters, Vol. 58, Issue 25 https://doi.org/10.1063/1.105227	journal	June 1991
Resolution and contrast in Kelvin probe force microscopy Jacobs, H. O.; Leuchtmann, P.; Homan, O. J. Journal of Applied Physics, Vol. 84, Issue 3 https://doi.org/10.1063/1.368181	journal	August 1998
Deposition and imaging of localized charge on insulator surfaces using a force microscope Stern, J. E.; Terris, B. D.; Mamin, H. J. Applied Physics Letters, Vol. 53, Issue 26 https://doi.org/10.1063/1.100162	journal	December 1988
Observation of single charge carriers by force microscopy Schönenberger, C.; Alvarado, S. F. Physical Review Letters, Vol. 65, Issue 25 https://doi.org/10.1103/PhysRevLett.65.3162	journal	December 1990
Conduction at domain walls in oxide multiferroics Seidel, J.; Martin, L. W.; He, Q. Nature Materials, Vol. 8, Issue 3 https://doi.org/10.1038/nmat2373	journal	January 2009
Deep Data Analysis of Conductive Phenomena on Complex Oxide Interfaces: Physics from Data Mining Strelcov, Evgheni; Belianinov, Alexei; Hsieh, Ying-Hui ACS Nano, Vol. 8, Issue 6 https://doi.org/10.1021/nn502029b	journal	May 2014
Scanning force microscopy of domain structure in ferroelectric thin films: imaging and control Gruverman, A.; Auciello, O.; Ramesh, R. Nanotechnology, Vol. 8, Issue 3A https://doi.org/10.1088/0957-4484/8/3A/008	journal	September 1997
Imaging and Control of Domain Structures in Ferroelectric thin Films via Scanning Force Microscopy Gruverman, Alexei; Auciello, Orlando; Tokumoto, Hiroshi Annual Review of Materials Science, Vol. 28, Issue 1 https://doi.org/10.1146/annurev.matsci.28.1.101	journal	August 1998
Piezoresponse force microscopy (PFM) Soergel, Elisabeth Journal of Physics D: Applied Physics, Vol. 44, Issue 46, Article No. 464003 https://doi.org/10.1088/0022-3727/44/46/464003	journal	November 2011
Local polarization dynamics in ferroelectric materials Kalinin, Sergei V.; Morozovska, Anna N.; Chen, Long Qing Reports on Progress in Physics, Vol. 73, Issue 5, Article No. 056502 https://doi.org/10.1088/0034-4885/73/5/056502	journal	April 2010
Scanning Thermal Microscopy Majumdar, A. Annual Review of Materials Science, Vol. 29, Issue 1 https://doi.org/10.1146/annurev.matsci.29.1.505	journal	August 1999
Scanning probe microscopy of thermal conductivity and subsurface properties Nonnenmacher, M.; Wickramasinghe, H. K. Applied Physics Letters, Vol. 61, Issue 2 https://doi.org/10.1063/1.108207	journal	July 1992
Ultrahigh-density atomic force microscopy data storage with erase capability Binnig, G.; Despont, M.; Drechsler, U. Applied Physics Letters, Vol. 74, Issue 9 https://doi.org/10.1063/1.123540	journal	March 1999
Temperature dependence of polarization and charge dynamics on the BaTiO3(100) surface by scanning probe microscopy Kalinin, Sergei V.; Bonnell, Dawn A. Applied Physics Letters, Vol. 78, Issue 8 https://doi.org/10.1063/1.1348303	journal	February 2001
Magnetic force microscopy characterization of a first-order transition: Magnetic-martensitic phase transformation in Gd[sub 5](Si[sub x]Ge[sub 1−x])[sub 4] Leib, J.; Snyder, J. E.; Lo, C. C. H. Journal of Applied Physics, Vol. 91, Issue 10 https://doi.org/10.1063/1.1456059	journal	January 2002
Direct Measurement of Thermoelastic Properties of Glassy and Rubbery Polymer Brush Nanolayers Grown by “Grafting-from” Approach Lemieux, M.; Minko, S.; Usov, D. Langmuir, Vol. 19, Issue 15 https://doi.org/10.1021/la0340504	journal	June 2003
Heat-assisted magnetic probe recording on a CoNi/Pt multilayered film Onoue, T.; Siekman, M. H.; Abelmann, L. Journal of Magnetism and Magnetic Materials, Vol. 287 https://doi.org/10.1016/j.jmmm.2004.10.083	journal	February 2005
Diffuse phase transition in BaTi1−xSnxO3 ceramics: An intermediate state between ferroelectric and relaxor behavior Shvartsman, V. V.; Kleemann, W.; Dec, J. Journal of Applied Physics, Vol. 99, Issue 12 https://doi.org/10.1063/1.2207828	journal	June 2006
Length-dependent thermal conductivity of an individual single-wall carbon nanotube Wang, Zhao Liang; Tang, Da Wei; Li, Xiao Bo Applied Physics Letters, Vol. 91, Issue 12 https://doi.org/10.1063/1.2779850	journal	September 2007
Evolution of nanodomains in 0.9PbMg1/3Nb2/3O3-0.1PbTiO3 single crystals Shvartsman, V. V.; Kholkin, A. L. Journal of Applied Physics, Vol. 101, Issue 6 https://doi.org/10.1063/1.2713084	journal	March 2007
Probing the temperature dependence of the mechanical properties of polymers at the nanoscale with band excitation thermal scanning probe microscopy Nikiforov, M. P.; Jesse, S.; Morozovska, A. N. Nanotechnology, Vol. 20, Issue 39 https://doi.org/10.1088/0957-4484/20/39/395709	journal	September 2009
Thermal probing of energy dissipation in current-carrying carbon nanotubes Shi, Li; Zhou, Jianhua; Kim, Philip Journal of Applied Physics, Vol. 105, Issue 10 https://doi.org/10.1063/1.3126708	journal	May 2009
Pyroelectric scanning probe microscopy: A method for local measurement of the pyroelectric effect in ferroelectric thin films Groten, J.; Zirkl, M.; Jakopic, G. Physical Review B, Vol. 82, Issue 5 https://doi.org/10.1103/PhysRevB.82.054112	journal	August 2010
Nanoscale Three-Dimensional Patterning of Molecular Resists by Scanning Probes Pires, D.; Hedrick, J. L.; De Silva, A. Science, Vol. 328, Issue 5979 https://doi.org/10.1126/science.1187851	journal	April 2010
Polarization reversal induced by heating-cooling cycles in MgO doped lithium niobate crystals Shur, V. Ya.; Mingaliev, E. A.; Lebedev, V. A. Journal of Applied Physics, Vol. 113, Issue 18 https://doi.org/10.1063/1.4801969	journal	May 2013
Intermittency, quasiperiodicity and chaos in probe-induced ferroelectric domain switching Ievlev, A. V.; Jesse, S.; Morozovska, A. N. Nature Physics, Vol. 10, Issue 1, p. 59-66 https://doi.org/10.1038/nphys2796	journal	November 2013
Ferroelectric domain inversion: The role of humidity Dahan, D.; Molotskii, M.; Rosenman, G. Applied Physics Letters, Vol. 89, Issue 15 https://doi.org/10.1063/1.2358855	journal	October 2006
Humidity effects on tip-induced polarization switching in lithium niobate Ievlev, A. V.; Morozovska, A. N.; Shur, V. Ya. Applied Physics Letters, Vol. 104, Issue 9 https://doi.org/10.1063/1.4867979	journal	March 2014
Direct visualization of the dynamic behavior of a water meniscus by scanning electron microscopy Schenk, Michael; Füting, Manfred; Reichelt, Rudolf Journal of Applied Physics, Vol. 84, Issue 9 https://doi.org/10.1063/1.368731	journal	November 1998
Ionic field effect and memristive phenomena in single-point ferroelectric domain switching Ievlev, Anton V.; Morozovska, Anna N.; Eliseev, Eugene A. Nature Communications, Vol. 5, Issue 1 https://doi.org/10.1038/ncomms5545	journal	July 2014
Ferrielectric ordering in lamellar ${CuInP}_{2} S_{6}$ Maisonneuve, V.; Cajipe, V. B.; Simon, A. Physical Review B, Vol. 56, Issue 17 https://doi.org/10.1103/PhysRevB.56.10860	journal	November 1997
Raman spectroscopy study of the ferrielectric-paraelectric transition in layered ${CuInP}_{2} S_{6}$ Vysochanskii, Yu. M.; Stephanovich, V. A.; Molnar, A. A. Physical Review B, Vol. 58, Issue 14 https://doi.org/10.1103/PhysRevB.58.9119	journal	October 1998
CuInP ₂ S ₆ Room Temperature Layered Ferroelectric Belianinov, A.; He, Q.; Dziaugys, A. Nano Letters, Vol. 15, Issue 6 https://doi.org/10.1021/acs.nanolett.5b00491	journal	May 2015
Superior Thermal Conductivity of Single-Layer Graphene Balandin, Alexander A.; Ghosh, Suchismita; Bao, Wenzhong Nano Letters, Vol. 8, Issue 3, p. 902-907 https://doi.org/10.1021/nl0731872	journal	March 2008
Measurement of porous silicon thermal conductivity by micro-Raman scattering Périchon, S.; Lysenko, V.; Remaki, B. Journal of Applied Physics, Vol. 86, Issue 8 https://doi.org/10.1063/1.371424	journal	October 1999
Electrical and thermal conductivity of low temperature CVD graphene: the effect of disorder Vlassiouk, Ivan; Smirnov, Sergei; Ivanov, Ilia Nanotechnology, Vol. 22, Issue 27 https://doi.org/10.1088/0957-4484/22/27/275716	journal	May 2011
Effects of pressure and temperature on the thermal conductivity of Sn $_{2}$ P $_{2}$ S $_{6}$ Andersson, O.; Chobal, O.; Rizak, I. Physical Review B, Vol. 83, Issue 13 https://doi.org/10.1103/PhysRevB.83.134121	journal	April 2011
Joint Bayesian Endmember Extraction and Linear Unmixing for Hyperspectral Imagery Dobigeon, N.; Moussaoui, S.; Coulon, M. IEEE Transactions on Signal Processing, Vol. 57, Issue 11 https://doi.org/10.1109/TSP.2009.2025797	journal	November 2009
Spectral mixture analysis of EELS spectrum-images Dobigeon, Nicolas; Brun, Nathalie Ultramicroscopy, Vol. 120 https://doi.org/10.1016/j.ultramic.2012.05.006	journal	September 2012
Principal component and spatial correlation analysis of spectroscopic-imaging data in scanning probe microscopy Jesse, Stephen; Kalinin, Sergei V. Nanotechnology, Vol. 20, Issue 8 https://doi.org/10.1088/0957-4484/20/8/085714	journal	February 2009
Multivariate statistical methods for the analysis of microscope image series: applications in materials science Bonnet, N. Journal of Microscopy, Vol. 190, Issue 1‐2 https://doi.org/10.1046/j.1365-2818.1998.3250876.x	journal	April 1998
Big data and deep data in scanning and electron microscopies: deriving functionality from multidimensional data sets Belianinov, Alex; Vasudevan, Rama; Strelcov, Evgheni Advanced Structural and Chemical Imaging, Vol. 1, Issue 1 https://doi.org/10.1186/s40679-015-0006-6	journal	May 2015

Cited By (6)

Tunable band alignment in two-phase-coexistence Nb ₃ O ₇ F nanocrystals with enhanced light harvesting and photocatalytic performance Li, Zhen; Huang, Fei; Feng, Xin Nanotechnology, Vol. 29, Issue 22 https://doi.org/10.1088/1361-6528/aab68e	journal	April 2018
Materials science in the artificial intelligence age: high-throughput library generation, machine learning, and a pathway from correlations to the underpinning physics Vasudevan, Rama K.; Choudhary, Kamal; Mehta, Apurva MRS Communications, Vol. 9, Issue 3 https://doi.org/10.1557/mrc.2019.95	journal	July 2019
Metal Thio- and Selenophosphates as Multifunctional van der Waals Layered Materials Susner, Michael A.; Chyasnavichyus, Marius; McGuire, Michael A. Advanced Materials, Vol. 29, Issue 38 https://doi.org/10.1002/adma.201602852	journal	August 2017
Machine learning-based multidomain processing for texture-based image segmentation and analysis Borodinov, Nikolay; Tsai, Wan-Yu; Korolkov, Vladimir V. Applied Physics Letters, Vol. 116, Issue 4 https://doi.org/10.1063/1.5135328	journal	January 2020
Graphene engineering by neon ion beams Iberi, Vighter; Ievlev, Anton V.; Vlassiouk, Ivan Nanotechnology, Vol. 27, Issue 12 https://doi.org/10.1088/0957-4484/27/12/125302	journal	February 2016
Automated Interpretation and Extraction of Topographic Information from Time of Flight Secondary Ion Mass Spectrometry Data Ievlev, Anton V.; Belianinov, Alexei; Jesse, Stephen Scientific Reports, Vol. 7, Issue 1 https://doi.org/10.1038/s41598-017-17049-y	journal	December 2017

Similar Records

Exploring Polarization Rotation Phase Instabilities in Super-Tetragonal BiFeO3 Epitaxial Thin Films and Their Technological Implications

Journal Article · Fri Jan 01 00:00:00 EST 2016 · Advanced Electronic Materials · OSTI ID:1237621

Cao, Ye; Yang, Mr. Shuzhen; Jesse, Stephen; +6 more

Giant negative electrostriction and dielectric tunability in a van der Waals layered ferroelectric

Journal Article · Fri Feb 01 00:00:00 EST 2019 · Physical Review Materials · OSTI ID:1237621

Neumayer, Sabine M.; Eliseev, Eugene A.; Susner, Michael A.; +11 more

Autonomous Experiments in Scanning Probe Microscopy and Spectroscopy: Choosing Where to Explore Polarization Dynamics in Ferroelectrics

Journal Article · Tue Jul 06 00:00:00 EDT 2021 · ACS Nano · OSTI ID:1237621

Vasudevan, Rama K.; Kelley, Kyle P.; Hinkle, Jacob; +4 more

Related Subjects

36 MATERIALS SCIENCE
77 NANOSCIENCE AND NANOTECHNOLOGY
ferroelectric
domain structure
scanning probe microscopy
piezoresponse forcr microscopy
Raman spectroscopy
phase transition
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Title: Quantitative analysis of the local phase transitions induced by the laser heating

Citation Formats

References (46)

Cited By (6)

Similar Records

Related Subjects