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Title: Process for manufacturing bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene

Abstract

A process to manufacture substituted tetracyano-hexaazatricyclics with the substitutions occurring at the 9 and 10 hydrogens. The process begins with 2,3-dichloro-5,6-dicyanopyrazine, which is reacted to form the desired tetracyano-hexaazatricyclic. Different process embodiments enable different reaction paths to the desired tetracyano-hexaazatricyclic. Different tetracyano-hexaazatricyclic embodiments include bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene and bis(2-methoxyethoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracen- e.

Inventors:
;
Publication Date:
Research Org.:
Vinazene, Inc., Ann Arbor, MI (USA)
Sponsoring Org.:
USDOE
OSTI Identifier:
1133643
Patent Number(s):
8,742,107
Application Number:
13/691,842
Assignee:
Vinazene, Inc. (Ann Arbor, MI)
DOE Contract Number:  
SC0007662
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats

Rasmussen, Paul George, and Lawton, Richard Graham. Process for manufacturing bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene. United States: N. p., 2014. Web.
Rasmussen, Paul George, & Lawton, Richard Graham. Process for manufacturing bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene. United States.
Rasmussen, Paul George, and Lawton, Richard Graham. 2014. "Process for manufacturing bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene". United States. https://www.osti.gov/servlets/purl/1133643.
@article{osti_1133643,
title = {Process for manufacturing bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene},
author = {Rasmussen, Paul George and Lawton, Richard Graham},
abstractNote = {A process to manufacture substituted tetracyano-hexaazatricyclics with the substitutions occurring at the 9 and 10 hydrogens. The process begins with 2,3-dichloro-5,6-dicyanopyrazine, which is reacted to form the desired tetracyano-hexaazatricyclic. Different process embodiments enable different reaction paths to the desired tetracyano-hexaazatricyclic. Different tetracyano-hexaazatricyclic embodiments include bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene and bis(2-methoxyethoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracen- e.},
doi = {},
url = {https://www.osti.gov/biblio/1133643}, journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Jun 03 00:00:00 EDT 2014},
month = {Tue Jun 03 00:00:00 EDT 2014}
}

Works referenced in this record:

Syntheses and spectral properties of 2,3,7,8-tetracyano-5,10-dihydrodipyrazino[2,3- b :2′,3′- e ]pyrazine
journal, March 1997


Polyazaacenes – On the Way to Stable, Fluorescent and Redox-Active Derivatives
journal, March 2007