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Title: Identification And Characterization Of The Solids Found In Extraction Contactor SEP-401 In June 2012

Technical Report ·
DOI:https://doi.org/10.2172/1084724· OSTI ID:1084724

The Modular Caustic-Side Solvent Extraction Unit (MCU) recently conducted an outage that included maintenance on the centrifugal contactors. Operations personnel observed solids or deposits in two contactors and attempted to collect samples for analyses by Savannah River National Laboratory (SRNL). The residues found in Extraction Contactor SEP-401 are a mixture of amorphous silica, aluminosilicate, titanium, and debris from low alloy steel. The solids contain low concentrations of plutonium and strontium. These isotopes are associated with the titanium that came from the monosodium titanate (MST) added in the Actinide Removal Process (ARP) most likely as leached Ti from the MST that precipitated subsequently in MCU. An attempt was also made to obtain samples from the contents of Wash Contactor SEP-702. However, sampling provide ineffective.

Research Organization:
Savannah River Site (SRS), Aiken, SC (United States)
Sponsoring Organization:
USDOE (United States)
DOE Contract Number:
DE-AC09-08SR22470
OSTI ID:
1084724
Report Number(s):
SRNL-STI-2012-00505; TRN: US1400061
Country of Publication:
United States
Language:
English