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Title: Preparation of membranes using solvent-less vapor deposition followed by in-situ polymerization

Patent ·
OSTI ID:1034644

A system of fabricating a composite membrane from a membrane substrate using solvent-less vapor deposition followed by in-situ polymerization. A first monomer and a second monomer are directed into a mixing chamber in a deposition chamber. The first monomer and the second monomer are mixed in the mixing chamber providing a mixed first monomer and second monomer. The mixed first monomer and second monomer are solvent-less vapor deposited onto the membrane substrate in the deposition chamber. The membrane substrate and the mixed first monomer and second monomer are heated to produce in-situ polymerization and provide the composite membrane.

Research Organization:
Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC52-07NA27344
Assignee:
Lawrence Livermore National Security, LLC (Livermore, CA)
Patent Number(s):
8,101,023
Application Number:
12/792,013
OSTI ID:
1034644
Country of Publication:
United States
Language:
English

References (1)

Solventless polyimide films by vapor deposition
  • Salem, J. R.; Sequeda, F. O.; Duran, J.
  • Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films, Vol. 4, Issue 3 https://doi.org/10.1116/1.573930
journal May 1986