Analytical Chemistry Laboratory (ACL) procedure compendium. Volume 3, Inorganic instrumental methods

Technical Report · Sun Aug 01 00:00:00 EDT 1993

DOI:https://doi.org/10.2172/10178513· OSTI ID:10178513

The methods cover: C in solutions, F (electrode), elements by atomic emission spectrometry, inorganic anions by ion chromatography, Hg in water/solids/sludges, As, Se, Bi, Pb, data calculations for SST (single shell tank?) samples, Sb, Tl, Ag, Pu, O/M ratio, ignition weight loss, pH value, ammonia (N), Cr(VI), alkalinity, U, C sepn. from soil/sediment/sludge, Pu purif., total N, water, C and S, surface Cl/F, leachable Cl/F, outgassing of Ge detector dewars, gas mixing, gas isotopic analysis, XRF of metals/alloys/compounds, H in Zircaloy, H/O in metals, inpurity extraction, reduced/total Fe in glass, free acid in U/Pu solns, density of solns, Kr/Xe isotopes in FFTF cover gas, H by combustion, MS of Li and Cs isotopes, MS of lanthanide isotopes, GC operation, total Na on filters, XRF spectroscopy QC, multichannel analyzer operation, total cyanide in water/solid/sludge, free cyanide in water/leachate, hydrazine conc., ICP-MS, {sup 99}Tc, U conc./isotopes, microprobe analysis of solids, gas analysis, total cyanide, H/N{sub 2}O in air, and pH in soil.

• Research Organization: Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
• Sponsoring Organization: USDOE, Washington, DC (United States)
• DOE Contract Number: AC06-76RL01830
• OSTI ID: 10178513
• Report Number(s): PNL-MA-599-Vol.3; ON: DE93019191; TRN: 93:019143
• Resource Relation: Other Information: PBD: [1993]
• Country of Publication: United States
• Language: English

Related Subjects

37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
BATTELLE PACIFIC NORTHWEST LABORATORIES
CHEMICAL ANALYSIS
MANUALS
MEASURING INSTRUMENTS
ELEMENTS
SPECTROSCOPY
PLUTONIUM
URANIUM
SOILS
SEDIMENTS
SLUDGES
CHLORIDES
FLUORIDES
GAS ANALYSIS
ISOTOPE RATIO
FLUORESCENCE SPECTROSCOPY
CYANIDES
MASS SPECTROSCOPY
TECHNETIUM 99
AIR
NITROUS OXIDE
PH VALUE
400102
400101
CHEMICAL AND SPECTRAL PROCEDURES
ACTIVATION, NUCLEAR REACTION, RADIOMETRIC, AND RADIOCHEMICAL PROCEDURES