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Title: Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama. Run 260 with Black Thunder Mine subbituminous coal: Technical progress report

Technical Report ·
DOI:https://doi.org/10.2172/10140954· OSTI ID:10140954

This report presents the results of Run 260 performed at the Advanced Coal Liquefaction R&D Facility in Wilsonville. The run was started on July 17, 1990 and continued until November 14, 1990, operating in the Close-Coupled Integrated Two-Stage Liquefaction mode processing Black Thunder mine subbituminous coal (Wyodak-Anderson seam from Wyoming Powder River Basin). Both thermal/catalytic and catalytic/thermal tests were performed to determine the methods for reducing solids buildup in a subbituminous coal operation, and to improve product yields. A new, smaller interstage separator was tested to reduce solids buildup by increasing the slurry space velocity in the separator. In order to obtain improved coal and resid conversions (compared to Run 258) full-volume thermal reactor and 3/4-volume catalytic reactor were used. Shell 324 catalyst, 1/16 in. cylindrical extrudate, at a replacement rate of 3 lb/ton of MF coal was used in the catalytic stage. Iron oxide was used as slurry catalyst at a rate of 2 wt % MF coal throughout the run. (TNPS was the sulfiding agent.)

Research Organization:
Southern Co. Services, Inc., Birmingham, AL (United States); Southern Electric International, Inc., Wilsonville, AL (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States); Electric Power Research Inst., Palo Alto, CA (United States)
DOE Contract Number:
AC22-90PC90033
OSTI ID:
10140954
Report Number(s):
DOE/PC/90033-16; ON: DE92013643
Resource Relation:
Other Information: PBD: Jan 1992
Country of Publication:
United States
Language:
English