System and method for liquid extraction electrospray-assisted sample transfer to solution for chemical analysis

Kertesz, Vilmos; Van Berkel, Gary J.

Title: System and method for liquid extraction electrospray-assisted sample transfer to solution for chemical analysis

Patent · Tue Jul 12 00:00:00 EDT 2016

OSTI ID:1261602

Kertesz, Vilmos; Van Berkel, Gary J.

A system for sampling a surface includes a surface sampling probe comprising a solvent liquid supply conduit and a distal end, and a sample collector for suspending a sample collection liquid adjacent to the distal end of the probe. A first electrode provides a first voltage to solvent liquid at the distal end of the probe. The first voltage produces a field sufficient to generate electrospray plume at the distal end of the probe. A second electrode provides a second voltage and is positioned to produce a plume-directing field sufficient to direct the electrospray droplets and ions to the suspended sample collection liquid. The second voltage is less than the first voltage in absolute value. A voltage supply system supplies the voltages to the first electrode and the second electrode. The first electrode can apply the first voltage directly to the solvent liquid. A method for sampling for a surface is also disclosed.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC05-00OR22725

Assignee:: UT-BATTELLE, LLC (Oak Ridge, TN)

Patent Number(s):: 9,390,901

Application Number:: 14/529,307

OSTI ID:: 1261602

Resource Relation:: Patent File Date: 2014 Oct 31

Country of Publication:: United States

Language:: English

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