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Title: Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples

Patent ·
OSTI ID:1257229
; ; ; ; ;

A magic-angle-spinning (MAS) nuclear magnetic resonance (NMR) probe is described that includes double containment enclosures configured to seal and contain hazardous samples for analysis. The probe is of a modular design that ensures containment of hazardous samples during sample analysis while preserving spin speeds for superior NMR performance and convenience of operation.

Research Organization:
Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC05-76RL01830
Assignee:
BATTELLE MEMORIAL INSTITUTE (Richland, WA)
Patent Number(s):
9,366,736
Application Number:
14/106,441
OSTI ID:
1257229
Resource Relation:
Patent File Date: 2013 Dec 13
Country of Publication:
United States
Language:
English

References (9)

Quantification of actinide α-radiation damage in minerals and ceramics journal January 2007
The aqueous complexation of thorium with citrate under neutral to basic conditions journal January 2006
Complexation of Cm(III)/Eu(III) with silicates in basic solutions journal January 2005
High-resolution solid-state nuclear magnetic resonance experiments on highly radioactive ceramics journal December 2004
Temperature and Isotope Substitution Effects on the Structure and NMR Properties of the Pertechnetate Ion in Water journal September 2004
Comprehensive Solid-State NMR Characterization of Electronic Structure in Ditechnetium Heptoxide journal September 2010
Method for the determination of very small magnetic susceptibilities and probehead for a high resolution nmr spectrometer for the purpose of carrying out the method patent June 1993
Polymeric NMR sample tubes and method for using patent July 2006
Apparatus for high-resolution NMR spectroscopy and/or imaging with an improved filling factor and RF field amplitude patent January 2012

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