Nuclear resonant inelastic X-ray scattering at high pressure and low temperature

Bi, Wenli; Zhao, Jiyong; Lin, Jung -Fu; Jia, Quanjie; Hu, Michael Y.; Jin, Changqing; Ferry, Richard; Yang, Wenge; Struzhkin, Viktor; Alp, E. Ercan

doi:10.1107/S1600577515003586

Title: Nuclear resonant inelastic X-ray scattering at high pressure and low temperature

Journal Article · Thu Jan 01 00:00:00 EST 2015 · Journal of Synchrotron Radiation (Online)

DOI:https://doi.org/10.1107/S1600577515003586· OSTI ID:1241005

Bi, Wenli ^[1]; Zhao, Jiyong ^[2]; Lin, Jung -Fu ^[3]; Jia, Quanjie ^[4]; Hu, Michael Y. ^[2]; Jin, Changqing ^[5]; Ferry, Richard ^[6]; Yang, Wenge ^[7]; Struzhkin, Viktor ^[8]; Alp, E. Ercan ^[2]

Univ. of Illinois at Urbana-Champaign, Urbana, IL (United States); Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
Univ. of Texas at Austin, Austin, TX (United States); Center for High Pressure Science and Technology Advanced Research (HPSTAR), Shanghai (China)
Chinese Academy of Sciences (CAS), Beijing (China). Inst. of High Energy Physics (IHEP)
Chinese Academy of Sciences (CAS), Beijing (China). Inst. of Physics
Carnegie Inst. of Washington, Argonne, IL (United States). HPSynC
Carnegie Inst. of Washington, Argonne, IL (United States). HPSynC; Center for High Pressure Science and Technology Advanced Research (HPSTAR), Shanghai (China)
Carnegie Inst. of Washington, Argonne, IL (United States). Geophysical Lab.

In this study, a new synchrotron radiation experimental capability of coupling nuclear resonant inelastic X-ray scattering with the cryogenically cooled high-pressure diamond anvil cell technique is presented. The new technique permits measurements of phonon density of states at low temperature and high pressure simultaneously, and can be applied to studies of phonon contribution to pressure- and temperature-induced magnetic, superconducting and metal–insulator transitions in resonant isotope-bearing materials. In this report, a pnictide sample, EuFe₂As₂, is used as an example to demonstrate this new capability at beamline 3-ID of the Advanced Photon Source, Argonne National Laboratory. A detailed description of the technical development is given. The Fe-specific phonon density of states and magnetism from the Fe sublattice in Eu⁵⁷Fe₂As₂ at high pressure and low temperature were derived by using this new capability.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC); National Science Foundation (NSF); National Natural Science Foundation of China (NSFC)

Grant/Contract Number:: AC02-06CH11357; EAR- 0838221; FG02- 99ER45775; 11220101003

OSTI ID:: 1241005

Journal Information:: Journal of Synchrotron Radiation (Online), Vol. 22, Issue 3; ISSN 1600-5775

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 13 works

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Cited By (5)

Magnetic phase diagram of $ɛ^{'}$ -FeH Ying, Jianjun; Zhao, Jiyong; Bi, Wenli Physical Review B, Vol. 101, Issue 2 https://doi.org/10.1103/physrevb.101.020405	journal	January 2020
Microscopic phase diagram of LaFeAsO single crystals under pressure Materne, Philipp; Bi, Wenli; Zhao, Jiyong Physical Review B, Vol. 98, Issue 17 https://doi.org/10.1103/physrevb.98.174510	journal	November 2018
High-pressure nuclear inelastic scattering with backscattering monochromatization Sergueev, Ilya; Glazyrin, Konstantin; Herrmann, Markus G. Journal of Synchrotron Radiation, Vol. 26, Issue 5 https://doi.org/10.1107/s1600577519008853	journal	August 2019
High-pressure nuclear inelastic scattering with backscattering monochromatization Sergueev, Ilya; Glazyrin, Konstantin; Herrmann, Markus G. Deutsches Elektronen-Synchrotron, DESY, Hamburg https://doi.org/10.3204/pubdb-2019-03277	text	January 2019
Microscopic phase diagram of LaFeAsO single crystals under pressure Materne, Philipp; Bi, Wenli; Zhao, Jiyong Unpublished https://doi.org/10.13140/rg.2.2.23533.23528	text	January 2018

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