Small nickel nanoparticle arrays from long chain imidazolium ionic liquids

Yang, Mei; Campbell, Paul S.; Santini, Catherine C.; Mudring, Anja -Verena

doi:10.1039/c3nr05048c

Title: Small nickel nanoparticle arrays from long chain imidazolium ionic liquids

Journal Article · Fri Nov 08 00:00:00 EST 2013 · Nanoscale

DOI:https://doi.org/10.1039/c3nr05048c· OSTI ID:1240909

Yang, Mei ^[1]; Campbell, Paul S. ^[1]; Santini, Catherine C. ^[2]; Mudring, Anja -Verena ^[3]

Ruhr-Univ. Bochum, Bochum (Germany)
Univ. de Lyon, Villeurbanne (France)
Ruhr-Univ. Bochum, Bochum (Germany); Iowa State Univ., Ames, IA (United States); Ames Lab., Ames, IA (United States)

A series of six long chain alkyl mono- and bi-cationic imidazolium based salts with bis(trifluoromethylsulfonyl)imide (NTf_2–) as the anion were synthesized and characterized. Single crystal structure of 1-methyl-3-octadecylimidazolium bis(trifluoromethylsulfonyl)imide could be obtained by X-ray analysis. All these long chain alkyl imidazolium based ILs were applied in the synthesis of nickel nanoparticles via chemical decomposition of an organometallic precursor of nickel. In these media, spontaneous decomposition of Ni(COD)₂ (COD = 1,5-cyclooctadiene) in the absence of H₂ occurred giving small NPs (≤4 nm) with narrow size distributions. Interestingly, formation of regularly interspaced NP arrays was also observed in long chain ILs. Lastly, such array formation could be interesting for potential applications such as carbon nanotube growth.

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Research Organization:: Ames Lab., Ames, IA (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC02-07CH11358

OSTI ID:: 1240909

Report Number(s):: IS-J-8295; NANOHL

Journal Information:: Nanoscale, Vol. 6, Issue 6; ISSN 2040-3364

Publisher:: Royal Society of ChemistryCopyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 39 works

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Aggregation control of Ru and Ir nanoparticles by tunable aryl alkyl imidazolium ionic liquids Schmolke, Laura; Lerch, Swantje; Bülow, Mark Nanoscale, Vol. 11, Issue 9 https://doi.org/10.1039/c8nr10286d	journal	January 2019
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