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Title: Tuning and synthesis of metallic nanostructures by mechanical compression

Patent ·
OSTI ID:1226011

The present invention provides a pressure-induced phase transformation process to engineer metal nanoparticle architectures and to fabricate new nanostructured materials. The reversible changes of the nanoparticle unit cell dimension under pressure allow precise control over interparticle separation in 2D or 3D nanoparticle assemblies, offering unique robustness for interrogation of both quantum and classic coupling interactions. Irreversible changes above a threshold pressure of about 8 GPa enables new nanostructures, such as nanorods, nanowires, or nanosheets.

Research Organization:
Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC04-94AL85000
Assignee:
Sandia Corporation
Patent Number(s):
9,180,420
Application Number:
13/905,965
OSTI ID:
1226011
Resource Relation:
Patent File Date: 2013 May 30
Country of Publication:
United States
Language:
English

References (5)

High pressure and low temperature sintering of nanophase ceramic powders patent May 2002
Self-assembly of water-soluble nanocrystals patent January 2012
Ordered Porous Mesotructured Materials from Nanoparticle-Block Copolymer Self Assembly patent-application June 2011
High-Pressure Structural Transformations in Semiconductor Nanocrystals journal October 1995
Pressure-induced morphology-dependent phase transformations of nanostructured tin dioxide journal September 2009