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Title: Synthesis of Propionamide Pyridine and Pyridine N-oxide Ligands

Journal Article · · Journal of Heterocyclic Chemistry, 44(1):99-103

A new set of pyridine and pyridine N-oxides functionalized with N,N-dimethylpropionamide pendant groups in the 2- and 2,6-positions have been prepared from the combination of 2-chloromethylpyridine and 2,6-bis(chloromethyl) pyridine with -lithio N,N-dimethyl acetamide. The coordination interaction between 2-(N,N-dimethylpropionamide) pyridine N-oxide (10) and Tb(NO3)3 has been unambiguously defined via single crystal X-ray diffraction analysis of Tb(10)(NO3)3(H2O). Battelle operates PNNL for the USDOE

Research Organization:
Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC05-76RL01830
OSTI ID:
903236
Report Number(s):
PNNL-SA-49118; KP1302000; TRN: US200719%%516
Journal Information:
Journal of Heterocyclic Chemistry, 44(1):99-103, Vol. 44, Issue 1
Country of Publication:
United States
Language:
English