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Title: Process for synthesis of beryllium chloride dietherate

A low temperature method of producing beryllium chloride dietherate through the addition of hydrogen chloride gas to a mixture of beryllium metal in ether in a reaction vessel is described. A reflux condenser provides an exit for hydrogen produced form the reaction. A distillation condenser later replaces the reflux condenser for purifying the resultant product.
Authors:
 [1] ;  [2] ;  [3]
  1. (Baton Rouge, LA)
  2. (Kendall Park, NJ)
  3. (Lynchburg, VA)
Publication Date:
OSTI Identifier:
867697
Report Number(s):
US 4990325
DOE Contract Number:
BNL-307348-S
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
process; synthesis; beryllium; chloride; dietherate; temperature; method; producing; beryllium; chloride; dietherate; addition; hydrogen; chloride; gas; mixture; beryllium; metal; reaction; vessel; described; reflux; condenser; provides; exit; hydrogen; produced; form; reaction; distillation; condenser; replaces; reflux; condenser; purifying; resultant; product; resultant product; reaction vessel; hydrogen chloride; reflux condenser; reflux condenser; hydrogen produced; chloride gas; chloride dietherate; chloride dietherate; temperature method; beryllium chloride; beryllium chloride /423/999/