Hydrotreating process employing a pretreated alumina containing material
This patent describes a hydrotreating process comprising the step of contacting a substantially liquid hydrocarbon-containing feed stream, which also contains compounds of at least one metal and/or sulfur as impurities, with a free hydrogen containing gas and a catalyst composition, under such conditions as to produce a hydrocarbon-containing stream having reduced levels of the at least one metal and sulfur; wherein the catalyst composition has been prepared by a process comprising the steps of (A) impregnating a support material comprising alumina with a solution consisting essentially of water and at least one dissolved thiocyanate compound; (B) heating the material obtained in step (A) under such conditions as to at least partially dry the material obtained in step (A); (C) impregnating the at least partially dried material obtained in step (B) with a solution comprising a liquid solvent and at least one dissolved compound of at least one metal selected from the group consisting of transition metals belonging to Group VB, VIB, Group VIIB, Group VIII and Group IB of the Periodic Table of Elements; (D) heating the material obtained in step (C) at a first temperature so as to least partially dry the material obtained in step (C); and (E) heating the at least partially dried material obtained in step (D) at a second temperature, which is higher than the first temperature, so as to activate at least partially dried material obtained in step (D).
- Assignee:
- Phillips Petroleum Co., Bartlesville, OK
- Patent Number(s):
- US 4778587
- OSTI ID:
- 6542422
- Resource Relation:
- Patent File Date: Filed date 20 May 1987
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
HYDROGENATION
CATALYSTS
PETROLEUM
ALUMINIUM OXIDES
CATALYST SUPPORTS
CHEMICAL COMPOSITION
CHEMICAL PREPARATION
CYANATES
HEATING
HYDROGEN
IMPURITIES
METALS
MIXING
SOLUTES
SULFUR CONTENT
THIOLS
WATER
ALUMINIUM COMPOUNDS
CARBONIC ACID DERIVATIVES
CHALCOGENIDES
CHEMICAL REACTIONS
ELEMENTS
ENERGY SOURCES
FOSSIL FUELS
FUELS
HYDROGEN COMPOUNDS
NITROGEN COMPOUNDS
NONMETALS
ORGANIC COMPOUNDS
ORGANIC SULFUR COMPOUNDS
OXIDES
OXYGEN COMPOUNDS
SYNTHESIS
020400* - Petroleum- Processing