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Title: Positron annihilation study on hafnium metals given various treatments

Journal Article · · Scripta Metallurgica et Materialia; (United States)
;  [1];  [2]
  1. Korea Atomic Energy Research Inst., Taejon (Korea, Republic of)
  2. Korea Advanced Inst. of Science and Tech., Taejon (Korea, Republic of)

The positron annihilation technique that enables measurements of positron lifetime, two-photon angular correlation and Doppler broadening due to annihilation radiation has been established for studies of the electronic configuration and defect properties in solids. In metals, positrons can be trapped at vacancies and their agglomerates as well as at dislocations, but not at interstitials. Because of these interactions, the positron annihilation method can be applied to studies of the behavior of dislocations during annealing of plastically deformed metals. Furthermore, it is possible by measurements of annihilation characteristics to identify defects such as vacancies, dislocations and vacancy-clusters, and to determine spatial dimensions of defects. In this work, positron annihilation measurements for annealed, cold worked, annealed and then quenched, and cold worked and then cathodically hydrogen charged hafnium specimens were made to obtain information on (a) positron annihilation characteristics of hafnium metal, (b) role of vacancy-type defects on hydrogen charging, (c) defects produced during hydrogen charging and (d) recovery of lattice defects in hafnium and effects of hydrogen on defects recovery upon annealing.

OSTI ID:
6354102
Journal Information:
Scripta Metallurgica et Materialia; (United States), Vol. 29:3; ISSN 0956-716X
Country of Publication:
United States
Language:
English