Epoxy resin cure. [Phenyl glycidyl ether]

Technical Report · Tue Jul 01 00:00:00 EDT 1986

OSTI ID:5533022

Smith, R E; Woodburn, G L

The reactions that occur between the model epoxy, phenyl glycidyl ether, and the cure agent dicyandiamide (DICY) have been investigated using nuclear magnetic resonance (NMR), Fourier transform infrared (FTIR), gel permeation chromatography (GPC), and high-performance liquid chromatography (HPLC) techniques. It is shown that the reaction at 130/sup 0/C requires 90 min for completion when catalyzed by boron trifluoride monoethyl amine (BF/sub 3/-MEA). At least three major products are formed. The identity of these products is based on previously published spectroscopic data. 3 refs., 5 figs.

• Research Organization: Allied Corp., Kansas City, MO (USA). Bendix Kansas City Div.
• DOE Contract Number: AC04-76DP00613
• OSTI ID: 5533022
• Report Number(s): BDX-613-3551; ON: DE86013613
• Resource Relation: Other Information: Portions of this document are illegible in microfiche products. Original copy available until stock is exhausted
• Country of Publication: United States
• Language: English

Related Subjects

37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
BORON FLUORIDES
CATALYTIC EFFECTS
CYANAMIDES
CHEMICAL REACTIONS
EPOXIDES
CURING
PHENYL ETHER
GEL PERMEATION CHROMATOGRAPHY
INFRARED SPECTRA
LIQUID COLUMN CHROMATOGRAPHY
NUCLEAR MAGNETIC RESONANCE
RESINS
EXPERIMENTAL DATA
HIGH TEMPERATURE
BORON COMPOUNDS
CARBONIC ACID DERIVATIVES
CHROMATOGRAPHY
DATA
ETHERS
FLUORIDES
FLUORINE COMPOUNDS
HALIDES
HALOGEN COMPOUNDS
INFORMATION
MAGNETIC RESONANCE
NUMERICAL DATA
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
ORGANIC OXYGEN COMPOUNDS
ORGANIC POLYMERS
PETROCHEMICALS
PETROLEUM PRODUCTS
POLYMERS
RESONANCE
SEPARATION PROCESSES
SPECTRA
400301* - Organic Chemistry- Chemical & Physicochemical Properties- (-1987)