Epoxy resin cure. [Phenyl glycidyl ether]
Abstract
The reactions that occur between the model epoxy, phenyl glycidyl ether, and the cure agent dicyandiamide (DICY) have been investigated using nuclear magnetic resonance (NMR), Fourier transform infrared (FTIR), gel permeation chromatography (GPC), and high-performance liquid chromatography (HPLC) techniques. It is shown that the reaction at 130/sup 0/C requires 90 min for completion when catalyzed by boron trifluoride monoethyl amine (BF/sub 3/-MEA). At least three major products are formed. The identity of these products is based on previously published spectroscopic data. 3 refs., 5 figs.
- Authors:
- Publication Date:
- Research Org.:
- Allied Corp., Kansas City, MO (USA). Bendix Kansas City Div.
- OSTI Identifier:
- 5533022
- Report Number(s):
- BDX-613-3551
ON: DE86013613
- DOE Contract Number:
- AC04-76DP00613
- Resource Type:
- Technical Report
- Resource Relation:
- Other Information: Portions of this document are illegible in microfiche products. Original copy available until stock is exhausted
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; BORON FLUORIDES; CATALYTIC EFFECTS; CYANAMIDES; CHEMICAL REACTIONS; EPOXIDES; CURING; PHENYL ETHER; GEL PERMEATION CHROMATOGRAPHY; INFRARED SPECTRA; LIQUID COLUMN CHROMATOGRAPHY; NUCLEAR MAGNETIC RESONANCE; RESINS; EXPERIMENTAL DATA; HIGH TEMPERATURE; BORON COMPOUNDS; CARBONIC ACID DERIVATIVES; CHROMATOGRAPHY; DATA; ETHERS; FLUORIDES; FLUORINE COMPOUNDS; HALIDES; HALOGEN COMPOUNDS; INFORMATION; MAGNETIC RESONANCE; NUMERICAL DATA; ORGANIC COMPOUNDS; ORGANIC NITROGEN COMPOUNDS; ORGANIC OXYGEN COMPOUNDS; ORGANIC POLYMERS; PETROCHEMICALS; PETROLEUM PRODUCTS; POLYMERS; RESONANCE; SEPARATION PROCESSES; SPECTRA; 400301* - Organic Chemistry- Chemical & Physicochemical Properties- (-1987)
Citation Formats
Smith, R E, and Woodburn, G L. Epoxy resin cure. [Phenyl glycidyl ether]. United States: N. p., 1986.
Web.
Smith, R E, & Woodburn, G L. Epoxy resin cure. [Phenyl glycidyl ether]. United States.
Smith, R E, and Woodburn, G L. 1986.
"Epoxy resin cure. [Phenyl glycidyl ether]". United States.
@article{osti_5533022,
title = {Epoxy resin cure. [Phenyl glycidyl ether]},
author = {Smith, R E and Woodburn, G L},
abstractNote = {The reactions that occur between the model epoxy, phenyl glycidyl ether, and the cure agent dicyandiamide (DICY) have been investigated using nuclear magnetic resonance (NMR), Fourier transform infrared (FTIR), gel permeation chromatography (GPC), and high-performance liquid chromatography (HPLC) techniques. It is shown that the reaction at 130/sup 0/C requires 90 min for completion when catalyzed by boron trifluoride monoethyl amine (BF/sub 3/-MEA). At least three major products are formed. The identity of these products is based on previously published spectroscopic data. 3 refs., 5 figs.},
doi = {},
url = {https://www.osti.gov/biblio/5533022},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Jul 01 00:00:00 EDT 1986},
month = {Tue Jul 01 00:00:00 EDT 1986}
}
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