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Title: Versatile magnetometer assembly for characterizing magnetic properties of nanoparticles

We constructed a versatile magnetometer assembly for characterizing iron oxide nanoparticles. The magnetometer can be operated at room temperature or inside a cryocooler at temperatures as low as 6 K. The magnetometer’s sensor can be easily exchanged and different detection electronics can be used. We tested the assembly with a non-cryogenic commercial Hall sensor and a benchtop multimeter in a four-wire resistance measurement scheme. A magnetic moment sensitivity of 8.5 × 10{sup −8} Am{sup 2} was obtained with this configuration. To illustrate the capability of the assembly, we synthesized iron oxide nanoparticles coated with different amounts of a triblock copolymer, Pluronic F-127, and characterized their magnetic properties. We determined that the polymer coating does not affect the magnetization of the particles at room temperature and demonstrates that it is possible to estimate the average size of coating layers from measurements of the magnetic field of the sample.
Authors:
; ;  [1]
  1. Department of Physics, Pontifícia Universidade Católica do Rio de Janeiro, Rio de Janeiro 22451-900 (Brazil)
Publication Date:
OSTI Identifier:
22482574
Resource Type:
Journal Article
Resource Relation:
Journal Name: Review of Scientific Instruments; Journal Volume: 86; Journal Issue: 10; Other Information: (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; COPOLYMERS; IRON OXIDES; MAGNETIC PROPERTIES; MAGNETOMETERS; NANOPARTICLES; SENSITIVITY; SENSORS; TEMPERATURE RANGE 0273-0400 K