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Title: Investigation of durability of optical coatings in highly purified tritium gas

Journal Article · · Fusion Science and Technology
DOI:https://doi.org/10.13182/FST14-T19· OSTI ID:22429706
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  1. Karlsruhe Institute of Technology - KIT, Karlsruhe (Germany)

Anti-reflection coated windows are part of Raman spectroscopy systems for tritium analytics in the KATRIN experiment and fusion-related applications. Damages of such windows were observed after three months of expo-sure to highly purified tritium gas in the LOOPINO facility. In this work, the origin of the damages was investigated, identified and eliminated. Coating samples manufactured by various physical vapor deposition methods have been tested for durability by exposure to pure tritium gas and subsequent visual inspection. Electron beam deposited coatings showed indications for damage after 17 days of tritium exposure in contrast to samples manufactured by ion assisted deposition or sputtering. An improved coating layout of the sample cell is presented for reliable long-term monitoring of tritium gas using Raman spectroscopy. (authors)

OSTI ID:
22429706
Journal Information:
Fusion Science and Technology, Vol. 67, Issue 2; Conference: TRITIUM 2013: 10. International Conference on Tritium Science and Technology, Nice Acropolis (France), 21-25 Oct 2013; Other Information: Country of input: France; 13 refs.; ISSN 1536-1055
Country of Publication:
United States
Language:
English