skip to main content

Title: Metallographic screening of grain boundary engineered type 304 austenitic stainless steel

An electrochemical etching method for the identification of grain boundary engineered type 304 austenitic stainless steel microstructures is described. The method can be applied for rapid microstructure screening to complement electron backscatter diffraction analysis. A threshold parameter to identify grain boundary engineered microstructure is proposed, and the application of metallographic etching for characterising the degree of grain boundary engineering discussed. - Highlights: • As-received (annealed) and grain boundary engineered microstructures were compared. • Electro-chemical polarisation in nitric acid solutions was carried out. • A metallographic screening method has been developed. • The screening method complements EBSD analysis for microstructure identification.
Authors:
;
Publication Date:
OSTI Identifier:
22403523
Resource Type:
Journal Article
Resource Relation:
Journal Name: Materials Characterization; Journal Volume: 94; Other Information: Copyright (c) 2014 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; BACKSCATTERING; COMPARATIVE EVALUATIONS; ELECTROCHEMISTRY; ELECTRON DIFFRACTION; ETCHING; GRAIN BOUNDARIES; METALLOGRAPHY; POLARIZATION; STAINLESS STEEL-304