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Title: Two-step fabrication technique of gold tips for use in point-contact spectroscopy

Journal Article · · Review of Scientific Instruments
DOI:https://doi.org/10.1063/1.4913661· OSTI ID:22392418
; ; ;  [1]
  1. Department of Physics and Material Research Laboratory, University of Illinois at Urbana-Champaign, Urbana, Illinois 61801 (United States)

For a successful point-contact spectroscopy (PCS) measurement, metallic tips of proper shape and smoothness are essential to ensure the ballistic nature of a point-contact junction. Until recently, the fabrication of Au tips suitable for use in point-contact spectroscopy has remained more of an art involving a trial and error method rather than an automated scientific process. To address these issues, we have developed a technique with which one can prepare high quality Au tips reproducibly and systematically. It involves an electronic control of the driving voltages used for an electrochemical etching of a gold wire in a HCl-glycerol mixture or a HCl solution. We find that a stopping current, below which the circuit is set to shut off, is a single very important parameter to produce an Au tip of desired shape. We present detailed descriptions for a two-step etching process for Au tips and also test results from PCS measurements using them.

OSTI ID:
22392418
Journal Information:
Review of Scientific Instruments, Vol. 86, Issue 3; Other Information: (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA); ISSN 0034-6748
Country of Publication:
United States
Language:
English