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Title: Structure analysis of O,O’-propane-1,3-diyl bis[diphenyl(phosphinothioate)]

A new diphosphine disulphide compound with the formula C{sub 27}H{sub 26}O{sub 2} vertical bar P{sub 2}S{sub 2}, was synthesized from the reaction between PPh{sub 2}SCl and 1,3-propanediol and characterized with different spectroscopic methods. Its structure has also been studied by X-ray diffraction. The compound crystallizes in the triclinic space group P-bar1. Pentavalent phosphorus atoms in the molecule are in distorted tetrahedral environments.
Authors:
;  [1] ;  [2]
  1. Ege University, Faculty of Science, Chemistry Department (Turkey)
  2. Ondokuz Mayıs University, Faculty of Science and Literature, Physics Department (Turkey)
Publication Date:
OSTI Identifier:
22311406
Resource Type:
Journal Article
Resource Relation:
Journal Name: Crystallography Reports; Journal Volume: 58; Journal Issue: 7; Other Information: Copyright (c) 2013 Pleiades Publishing, Inc.; http://www.springer-ny.com; Country of input: International Atomic Energy Agency (IAEA)
Country of Publication:
United States
Language:
English
Subject:
75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; 36 MATERIALS SCIENCE; ALKYL RADICALS; PHENYLENE RADICALS; PHOSPHORUS; PROPANE; SPACE GROUPS; STRUCTURAL CHEMICAL ANALYSIS; X-RAY DIFFRACTION